比索洛尔左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.211037481038061036421036071035941036790.09
214.121034701034951034820.02
单位质量响应值RSD%判断
7296.207328.750.32数据可信
供试品溶液-8145795批-shui
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146936-4693640.52640.446.4240.5340.446.42
245431-4543139.22739.23
352236-5223645.10245.10
443560-4356037.61137.61
547616-4761641.11341.11
645209-4520939.03539.03
10min171892-7189262.07458.896.1462.1458.966.14
269948-6994860.39560.46
373066-7306663.08863.16
467432-6743258.22358.29
564299-6429955.51855.59
662587-6258754.04054.10
15min177450-7745066.87366.003.4167.0466.163.40
277213-7721366.66866.83
376864-7686466.36766.55
471495-7149561.73161.89
579194-7919468.37968.54
676412-7641265.97766.13
20min181545-8154570.40970.572.1870.6970.842.19
281263-8126370.16570.44
384866-8486673.27673.57
479387-7938768.54568.81
581293-8129370.19170.47
682031-8203170.82871.09
30min185544-8554473.86173.433.8974.2673.823.88
282991-8299171.65772.05
390652-9065278.27278.68
484201-8420172.70273.08
580895-8089569.84770.24
685952-8595274.21474.60
45min190981-9098178.55680.162.5879.0880.682.58
293802-9380280.99281.51
396721-9672183.51284.06
490265-9026577.93878.44
593698-9369880.90281.41
691540-9154079.03979.55
极限1110323-11032395.25694.743.0695.9195.393.04
2104727-10472790.42591.07
3114071-11407198.49399.18
4111953-11195396.66497.29
5110112-11011295.07495.72
6107142-10714292.51093.15
比索洛尔左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.211036301036271034821034991037691036010.12
214.121036881037981037430.08
单位质量响应值RSD%判断
7290.717347.240.55数据可信
供试品溶液-8145795批-shui
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144936-4493638.76539.3317.2838.7739.3317.28
249745-4974542.91442.91
345531-4553139.27839.28
431875-3187527.49827.50
545653-4565339.38439.38
655803-5580348.14048.14
10min168349-6834958.96358.779.9959.0358.8410.00
269998-6999860.38560.46
370763-7076361.04561.11
455027-5502747.47047.52
569613-6961360.05360.12
674995-7499564.69664.78
15min176890-7689066.33166.128.0866.4966.288.09
272796-7279662.79962.97
376398-7639865.90766.07
467422-6742258.16358.29
581459-8145970.27370.44
684916-8491673.25573.44
20min181636-8163670.42570.146.3370.7070.426.34
280206-8020669.19269.47
380164-8016469.15569.43
472708-7270862.72362.95
586280-8628074.43274.71
686852-8685274.92575.24
30min185699-8569973.93073.545.0774.3273.925.09
284889-8488973.23273.62
382045-8204570.77871.17
479027-7902768.17568.50
590586-9058678.14678.55
689198-8919876.94977.38
45min192570-9257079.85879.397.2580.3779.907.25
291864-9186479.24979.76
393633-9363380.77581.29
479369-7936968.47068.91
596414-9641483.17483.71
698327-9832784.82485.39
极限1108871-10887193.92094.594.4594.5795.244.45
2103362-10336289.16889.81
3112532-11253297.07897.72
4104804-10480490.41290.97
5115929-115929100.009100.68
6112385-11238596.95297.66
比索洛尔左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.211036811037041036651036141035661036460.06
214.121036481035361035920.08
单位质量响应值RSD%判断
7293.887336.540.42数据可信
供试品溶液-8145795批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min194916-9491681.92380.142.2381.9280.142.23
294826-9482681.84681.85
391669-9166979.12179.12
494056-9405681.18181.18
589809-8980977.51577.52
691800-9180079.23479.23
10min1109146-10914694.20591.521.6694.3491.651.66
2104538-10453890.22890.36
3105914-10591491.41691.55
4106532-10653291.94992.08
5105854-10585491.36491.49
6104232-10423289.96490.10
15min1113874-11387498.28694.921.9098.5895.211.90
2107885-10788593.11793.40
3110008-11000894.94995.23
4110202-11020295.11795.41
5109048-10904894.12194.40
6108840-10884093.94194.22
20min1116132-116132100.23596.542.12100.6996.982.11
2109639-10963994.63195.07
3111866-11186696.55397.00
4112352-11235296.97297.42
5111278-11127896.04596.48
6109828-10982894.79495.23
30min1117170-117170101.13197.852.03101.7698.452.03
2111586-11158696.31196.91
3113441-11344197.91298.52
4114448-11444898.78299.39
5112882-11288297.43098.03
6110655-11065595.50896.10
45min1118902-118902102.62698.652.17103.4299.422.17
2112642-11264297.22397.98
3114708-11470899.00699.77
4113949-11394998.35199.12
5113765-11376598.19298.95
6111837-11183796.52897.28
极限1118903-118903102.62798.502.41103.5999.442.41
2111717-11171796.42497.35
3114418-11441898.75699.69
4114772-11477299.061100.00
5113721-11372198.15499.08
6111216-11121695.99296.91
比索洛尔左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.211035381035361035711036751036241035890.06
214.121036391036711036550.03
单位质量响应值RSD%判断
7289.877341.010.50数据可信
供试品溶液-8145795批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min190992-9099278.53480.033.7678.5380.023.76
292808-9280880.10280.10
398880-9888085.34285.34
488419-8841976.31376.31
593354-9335480.57380.57
691876-9187679.29779.30
10min1106043-10604391.52592.242.5991.6692.382.60
2105386-10538690.95891.09
3112416-11241697.02597.17
4104966-10496690.59590.72
5106501-10650191.92092.05
6105950-10595091.44491.58
15min1109362-10936294.38995.351.9694.6795.641.96
2109027-10902794.10094.39
3114476-11447698.80399.11
4108537-10853793.67793.96
5110974-11097495.78096.07
6110447-11044795.32695.61
20min1111459-11145996.19996.601.7896.6497.041.78
2109932-10993294.88195.32
3115470-11547099.661100.13
4110256-11025695.16195.60
5112336-11233696.95697.40
6112086-11208696.74097.18
30min1112819-11281997.37397.691.6697.9798.301.67
2110917-11091795.73196.33
3116279-116279100.359100.99
4112178-11217896.82097.41
5114354-11435498.69899.31
6112582-11258297.16897.77
45min1113490-11349097.95298.211.4798.7298.981.48
2112395-11239597.00797.77
3117008-117008100.988101.79
4112570-11257097.15897.91
5113828-11382898.24499.02
6113471-11347197.93698.70
极限1115218-11521899.44398.491.53100.3799.421.53
2112509-11250997.10598.03
3116227-116227100.314101.28
4112981-11298197.51398.43
5115532-11553299.714100.65
6112219-11221996.85597.78
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