盐酸鲁拉西酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号N877-220209对照品来源自制对照品使用方法直接使用
对照品含量(%)99.74对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.111958601959421954381956471956311957040.11
211.151969721965781967750.15
单位质量响应值RSD%判断
17615.1217647.980.14数据可信
供试品溶液-24051001批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min186923-8692344.25447.956.5444.2547.956.55
298611-9861150.20550.21
388079-8807944.84344.84
492266-9226646.97546.97
596590-9659049.17649.18
6102583-10258352.22752.23
10min1138098-13809870.30972.042.1370.3872.122.13
2144633-14463373.63673.72
3137899-13789970.20770.28
4143187-14318772.90072.98
5140921-14092171.74671.83
6144250-14425073.44173.53
15min1160247-16024781.58582.140.8881.7882.340.89
2162088-16208882.52382.73
3160043-16004381.48181.67
4160390-16039081.65881.86
5161537-16153782.24282.44
6163723-16372383.35583.56
20min1173306-17330688.23488.461.3988.5688.801.40
2178063-17806390.65691.00
3171893-17189387.51487.84
4171877-17187787.50687.84
5172390-17239087.76888.11
6174981-17498189.08789.44
30min1182836-18283693.08693.440.5893.5693.920.59
2183350-18335093.34793.84
3183444-18344493.39593.87
4183207-18320793.27593.76
5182701-18270193.01793.50
6185604-18560494.49594.99
45min1189858-18985896.66196.780.4397.2997.420.43
2189574-18957496.51697.17
3190099-19009996.78497.41
4190104-19010496.78697.42
5189293-18929396.37397.01
6191624-19162497.56098.21
60min1191405-19140597.44897.870.5298.2498.670.52
2191645-19164597.57198.38
3193127-19312798.32599.12
4192479-19247997.99598.79
5191178-19117897.33398.13
6193597-19359798.56499.38
极限1192939-19293998.22998.360.5599.1899.320.55
2192164-19216497.83598.81
3194529-19452999.03999.99
4192698-19269898.10799.07
5192323-19232397.91698.88
6194480-19448099.014100.00
盐酸鲁拉西酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号N877-220209对照品来源自制对照品使用方法直接使用
对照品含量(%)99.74对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.111958991960371962241956231959981959560.12
211.151974441974591974520.01
单位质量响应值RSD%判断
17637.8017708.700.29数据可信
供试品溶液-24051001批-pH3.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1105545-10554553.60950.975.3853.6150.975.38
2104666-10466653.16253.16
3103021-10302152.32752.33
493381-9338147.43047.43
593839-9383947.66347.66
6101668-10166851.63951.64
10min1141008-14100871.62168.454.0871.7168.544.08
2139897-13989771.05771.15
3136974-13697469.57269.66
4126800-12680064.40564.48
5131179-13117966.62966.71
6132751-13275167.42767.51
15min1157515-15751580.00577.143.0380.2177.343.03
2155307-15530778.88479.09
3154514-15451478.48178.68
4145701-14570174.00574.19
5149818-14981876.09676.29
6148359-14835975.35575.55
20min1165437-16543784.02982.032.3184.3782.362.31
2164597-16459783.60283.94
3163478-16347883.03483.37
4156461-15646179.47079.78
5161378-16137881.96782.28
6157656-15765680.07780.40
30min1174826-17482688.79887.621.9389.2888.081.93
2175938-17593889.36389.84
3174684-17468488.72689.20
4168262-16826285.46485.91
5172676-17267687.70688.16
6168612-16861285.64286.10
45min1183940-18394093.42792.341.2794.0692.951.28
2182809-18280992.85393.48
3183689-18368993.30093.92
4178998-17899890.91791.50
5182535-18253592.71493.31
6178790-17879090.81191.41
60min1188553-18855395.77094.811.0096.5695.581.01
2186708-18670894.83395.61
3188699-18869995.84496.62
4185165-18516594.04994.79
5186898-18689894.93095.68
6183964-18396493.43994.19
极限1193304-19330498.18397.380.7799.1398.300.78
2191526-19152697.28098.22
3193117-19311798.08899.02
4190112-19011296.56297.45
5192316-19231697.68298.59
6189933-18993396.47197.38
盐酸鲁拉西酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号N877-220209对照品来源自制对照品使用方法直接使用
对照品含量(%)99.74对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.111988441992041988761990841989061989830.08
211.151976881974061975470.11
单位质量响应值RSD%判断
17910.2617717.220.77数据可信
供试品溶液-24051001批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min178521-7852139.56940.413.4939.5740.413.49
282249-8224941.44841.45
375666-7566638.13038.13
481203-8120340.92140.92
580031-8003140.33040.33
683417-8341742.03642.04
10min1109206-10920655.03255.782.2655.1055.842.26
2112881-11288156.88456.95
3106416-10641653.62653.69
4111939-11193956.40956.48
5110932-11093255.90255.97
6112736-11273656.81156.88
15min1126219-12621963.60564.391.7363.7664.541.74
2128685-12868564.84865.01
3124065-12406562.52062.67
4128346-12834664.67764.84
5129524-12952465.27165.43
6129776-12977665.39865.56
20min1137403-13740369.24170.271.7369.5170.541.73
2140043-14004370.57270.84
3135975-13597568.52268.78
4140449-14044970.77671.05
5140068-14006870.58470.85
6142764-14276471.94372.22
30min1150341-15034175.76176.701.3776.1477.091.38
2152932-15293277.06777.46
3148953-14895375.06275.43
4153121-15312177.16277.55
5154176-15417677.69478.08
6153753-15375377.48177.87
45min1162310-16231081.79382.720.9682.3083.240.96
2164547-16454782.92083.44
3162050-16205081.66282.16
4165516-16551683.40883.92
5165054-16505483.17683.69
6165446-16544683.37383.90
60min1170069-17006985.70386.360.7786.3487.010.78
2171909-17190986.63087.29
3169585-16958585.45986.09
4171535-17153586.44187.10
5173088-17308887.22487.88
6172064-17206486.70887.37
极限1179312-17931290.36191.211.0191.1592.011.01
2181683-18168391.55592.36
3178180-17818089.79090.57
4181967-18196791.69892.50
5182682-18268292.05992.86
6182199-18219991.81592.62
盐酸鲁拉西酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号N877-220209对照品来源自制对照品使用方法直接使用
对照品含量(%)99.74对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.111964331965391962791961171958831962500.14
211.151992341994771993560.09
单位质量响应值RSD%判断
17664.2717879.460.86数据可信
供试品溶液-24051001批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min139014-3901419.70716.2813.4319.7116.2813.43
228586-2858614.43914.44
334603-3460317.47917.48
426977-2697713.62713.63
532852-3285216.59416.59
631355-3135515.83815.84
10min157894-5789429.24325.678.9529.2825.708.97
247256-4725623.87023.89
354356-5435627.45627.49
445983-4598323.22723.25
550792-5079225.65625.68
648656-4865624.57724.60
15min167735-6773534.21431.386.2834.3031.456.30
259366-5936629.98730.05
365739-6573933.20633.28
457568-5756829.07929.14
561921-6192131.27831.35
660376-6037630.49730.56
20min173497-7349737.12534.774.7437.2634.904.75
266847-6684733.76633.88
371881-7188136.30936.44
465501-6550133.08633.20
569132-6913234.92035.04
666194-6619433.43633.55
30min180133-8013340.47738.773.5240.6838.963.54
275600-7560038.18738.36
379417-7941740.11540.31
473726-7372637.24037.41
577543-7754339.16939.35
674135-7413537.44737.62
45min185211-8521143.04241.792.1943.3142.032.22
281497-8149741.16641.40
384262-8426242.56242.82
481000-8100040.91541.14
583373-8337342.11342.36
681012-8101240.92141.16
60min187730-8773044.31443.391.7944.6543.701.81
285162-8516243.01743.32
387513-8751344.20544.53
484388-8438842.62642.92
586389-8638943.63743.95
684256-8425642.55942.86
极限189657-8965745.28844.591.4245.7044.981.45
287970-8797044.43544.81
389651-8965145.28545.69
486487-8648743.68644.05
588416-8841644.66145.05
687465-8746544.18044.56
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2024-05-16 15:24:37 完成)
生成报告数据部分下载报告(谢超君 于 2024-05-16 15:25:06 完成)
Current page cost:71 ms