叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.191010731011381011121011801008411010690.14
210.191007691005441006560.16
单位质量响应值RSD%判断
9918.459877.920.29数据可信
供试品溶液-24050901批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min18246-824613.67613.9711.6013.6813.9711.59
210088-1008816.73116.73
38873-887314.71614.72
47541-754112.50712.51
57435-743512.33112.33
68343-834313.83713.84
10min116138-1613826.76526.236.5626.9226.386.59
217504-1750429.03029.22
316037-1603726.59726.76
414424-1442423.92224.06
515571-1557125.82425.96
615204-1520425.21625.37
15min119775-1977532.79732.756.7433.2533.206.75
222021-2202136.52237.03
320324-2032433.70734.17
418171-1817130.13630.54
519012-1901231.53131.96
619189-1918931.82532.26
20min122728-2272837.69437.426.5738.5138.236.57
225213-2521341.81642.73
321779-2177936.12036.95
420760-2076034.43035.17
522366-2236637.09437.87
622536-2253637.37638.16
30min127497-2749745.60444.944.6846.8446.174.72
229481-2948148.89450.27
326712-2671244.30245.54
426590-2659044.09945.22
526102-2610243.29044.48
626211-2621143.47144.67
45min131133-3113351.63450.125.1753.3751.855.19
232444-3244453.80855.73
330441-3044150.48652.21
427900-2790046.27247.88
529227-2922748.47350.14
630193-3019350.07551.76
60min133166-3316655.00653.795.6657.3256.075.65
235534-3553458.93361.45
331730-3173052.62454.91
430226-3022650.13052.26
531313-3131351.93254.14
632619-3261954.09856.34
90min137372-3737261.98160.627.2164.9163.507.14
241006-4100668.00871.18
336372-3637260.32363.20
433470-3347055.51058.19
534405-3440557.06059.84
636673-3667360.82263.67
极限140312-4031266.85766.478.5770.4770.038.44
245897-4589776.12080.05
340595-4059567.32770.87
435435-3543558.76962.07
538297-3829763.51566.93
639949-3994966.25569.77
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.191006251008361008691005661006341007060.14
210.191008821007991008400.06
单位质量响应值RSD%判断
9882.839895.980.10数据可信
供试品溶液-24050902批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17773-777312.90313.544.3112.9013.544.32
28529-852914.15814.16
38037-803713.34113.34
47960-796013.21313.21
57994-799413.27013.27
68659-865914.37414.37
10min114158-1415823.50223.984.3623.6524.144.34
213979-1397923.20523.36
315227-1522725.27625.42
413888-1388823.05423.20
514168-1416823.51823.67
615272-1527225.35125.51
15min118663-1866330.98030.674.1531.3831.094.12
218462-1846230.64631.06
319595-1959532.52732.96
417821-1782129.58229.99
517447-1744728.96129.37
618869-1886931.32231.76
20min121640-2164035.92235.392.7136.6736.142.72
221231-2123135.24336.00
321991-2199136.50437.29
420692-2069234.34835.08
520599-2059934.19434.92
621749-2174936.10236.89
30min124976-2497641.45941.414.0742.6142.574.03
225147-2514741.74342.89
326610-2661044.17245.37
424321-2432140.37241.49
523563-2356339.11440.22
625076-2507641.62542.82
45min128539-2853947.37448.275.5348.9849.885.44
230429-3042950.51152.12
331259-3125951.88953.58
428314-2831447.00048.56
526750-2675044.40445.95
629178-2917848.43450.09
60min131968-3196853.06653.586.3255.2055.736.21
234462-3446257.20659.38
334759-3475957.69959.96
431110-3111051.64153.73
529396-2939648.79650.83
631972-3197253.07255.26
90min135827-3582759.47160.226.7462.2062.966.62
238921-3892164.60767.42
338898-3889864.56967.47
435192-3519258.41761.08
532453-3245353.87156.45
636362-3636260.35963.14
极限139777-3977766.02866.288.0969.4169.707.90
243705-4370572.54976.07
344004-4400473.04576.67
437241-3724161.81965.13
536561-3656160.69063.87
638294-3829463.56667.02
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.191009791010421011261010311009691010290.07
210.191005471008551007010.22
单位质量响应值RSD%判断
9914.529882.340.23数据可信
供试品溶液-24050903批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min16911-691111.46213.4211.5011.4613.4211.51
26930-693011.49311.49
38290-829013.74913.75
48823-882314.63214.63
58816-881614.62114.62
68789-878914.57614.58
10min112489-1248920.71224.7010.2120.8424.8510.21
213877-1387723.01423.14
315283-1528325.34625.50
416862-1686227.96528.13
515172-1517225.16225.32
615688-1568826.01826.18
15min117394-1739428.84731.264.9729.2031.685.02
218865-1886531.28731.67
318694-1869431.00331.44
420325-2032533.70834.18
518744-1874431.08631.53
619078-1907831.64032.09
20min119649-1964932.58735.475.2933.2636.245.32
221654-2165435.91236.64
321595-2159535.81436.59
423050-2305038.22739.08
520742-2074234.40035.19
621640-2164035.88936.69
30min123688-2368839.28541.396.7640.3342.566.69
225158-2515841.72342.85
325926-2592642.99744.17
427693-2769345.92747.20
523065-2306538.25239.42
624219-2421940.16641.37
45min128557-2855747.36046.887.0048.8448.506.82
228730-2873047.64749.24
324629-2462940.84642.50
430694-3069450.90452.69
528356-2835647.02748.62
628621-2862147.46649.11
60min131805-3180552.74753.774.6954.7555.924.58
233414-3341455.41557.54
334077-3407756.51558.62
433556-3355655.65158.00
530078-3007849.88352.00
631612-3161252.42754.60
90min135639-3563959.10561.274.4361.6964.014.34
238743-3874364.25366.99
338551-3855163.93566.67
437948-3794862.93565.90
535485-3548558.85061.52
635293-3529358.53261.29
极限138654-3865464.10665.764.7767.3569.184.62
241830-4183069.37372.83
341958-4195869.58573.03
439819-3981966.03869.70
537956-3795662.94866.27
637674-3767462.48065.89
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