替米沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.113880513871633880373875303873733876310.11
211.033897503895513896500.04
单位质量响应值RSD%判断
34890.2835326.380.88数据可信
供试品溶液-24041801批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min135172-351729.0179.0812.539.029.0812.53
229389-293897.5347.53
342836-4283610.98110.98
436885-368859.4569.46
534807-348078.9238.92
633340-333408.5478.55
10min191429-9142923.43924.422.7423.4924.472.73
293438-9343823.95424.00
394706-9470624.27924.34
496109-9610924.63824.69
597320-9732024.94925.00
698522-9852225.25725.30
15min1131871-13187133.80634.422.1233.9934.612.12
2132105-13210533.86634.04
3131901-13190133.81434.01
4134346-13434634.44134.63
5137325-13732535.20535.39
6138155-13815535.41735.61
20min1153809-15380939.43040.603.6739.8040.983.65
2151643-15164338.87539.24
3154312-15431239.55939.94
4162194-16219441.58041.96
5162472-16247241.65142.03
6165768-16576842.49642.88
30min1170041-17004143.59244.821.7844.1845.431.78
2172641-17264144.25844.84
3178460-17846045.75046.35
4174498-17449844.73445.35
5176673-17667345.29245.91
6176732-17673245.30745.93
45min1180285-18028546.21847.171.2947.0548.021.28
2185733-18573347.61448.44
3185607-18560747.58248.44
4182531-18253146.79447.65
5183272-18327246.98347.85
6186457-18645747.80048.67
60min1176429-17642945.22946.031.6946.3247.141.69
2176307-17630745.19846.29
3177841-17784145.59146.71
4181435-18143546.51347.63
5182463-18246346.77647.90
6182827-18282746.86948.01
极限1183010-18301046.91646.902.3548.2548.272.28
2182471-18247146.77848.12
3175811-17581145.07146.45
4186128-18612847.71649.09
5188391-18839148.29649.68
6181916-18191646.63648.03
替米沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.113849083852333855393851333854593852540.07
211.033845073857333851200.23
单位质量响应值RSD%判断
34676.3334915.680.49数据可信
供试品溶液-24041801批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min139317-3931710.1699.5211.9710.179.5211.95
231838-318388.2358.24
340326-4032610.43010.43
434463-344638.9148.91
532540-325408.4178.42
642268-4226810.93310.93
10min1104102-10410226.92626.274.2226.9826.324.24
299832-9983225.82225.87
3103036-10303626.65126.71
498064-9806425.36525.41
596394-9639424.93324.98
6107977-10797727.92927.99
15min1149445-14944538.65437.073.1238.8637.273.12
2141061-14106136.48636.68
3142894-14289436.96037.17
4137043-13704335.44735.64
5142146-14214636.76736.95
6147334-14733438.10838.32
20min1166349-16634943.02743.252.2143.4543.662.21
2163209-16320942.21542.61
3166248-16624843.00143.41
4164345-16434542.50842.90
5170323-17032344.05544.44
6172904-17290444.72245.15
30min1180097-18009746.58345.103.3747.2445.743.30
2175025-17502545.27145.90
3176434-17643445.63546.29
4175642-17564245.43046.05
5175988-17598845.52046.15
6162942-16294242.14642.82
45min1183708-18370847.51748.321.3048.4449.221.25
2189511-18951149.01849.90
3188427-18842748.73749.64
4188877-18887748.85449.73
5184742-18474247.78448.67
6185704-18570448.03348.94
60min1182642-18264247.24147.701.2648.4248.861.22
2181557-18155746.96048.11
3184254-18425447.65848.83
4188228-18822848.68649.83
5184371-18437147.68848.84
6185430-18543047.96249.14
极限1188274-18827448.69847.911.2050.1449.341.16
2185216-18521647.90749.32
3181770-18177047.01548.45
4186786-18678648.31349.73
5184761-18476147.78949.21
6184583-18458347.74349.19
替米沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.113869583875173871203873153876403873100.08
211.033926993921033924010.11
单位质量响应值RSD%判断
34861.3935575.791.44数据可信
供试品溶液-24041901批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min181735-8173520.88918.449.6520.8918.449.65
277642-7764219.84319.84
366414-6641416.97416.97
465572-6557216.75816.76
575280-7528019.24019.24
666316-6631616.94916.95
10min1111515-11151528.50026.829.5828.6226.939.55
2119305-11930530.49130.60
3107560-10756027.48927.58
4103195-10319526.37426.47
596132-9613224.56924.68
691999-9199923.51223.61
15min1139089-13908935.54734.894.9135.8235.144.92
2147976-14797637.81938.10
3134971-13497134.49534.74
4136143-13614334.79435.03
5128191-12819132.76233.01
6132694-13269433.91334.14
20min1158875-15887540.60440.093.0341.0840.533.05
2161087-16108741.17041.66
3161547-16154741.28741.73
4155227-15522739.67240.10
5148861-14886138.04538.47
6155479-15547939.73640.15
30min1174389-17438944.56944.312.0245.2744.981.99
2170645-17064543.61244.33
3177007-17700745.23845.91
4176007-17600744.98345.64
5167778-16777842.88043.52
6174524-17452444.60445.24
45min1161216-16121641.20245.174.5242.1546.094.41
2179968-17996845.99546.96
3184356-18435647.11648.04
4177162-17716245.27846.18
5178817-17881745.70146.58
6178916-17891645.72646.61
60min1172133-17213343.99344.681.9345.1745.841.91
2175813-17581344.93346.15
3178520-17852045.62546.81
4174770-17477044.66745.82
5169787-16978743.39344.52
6177898-17789845.46646.60
极限1170066-17006643.46444.952.8144.8846.372.69
2177143-17714345.27346.74
3174402-17440244.57246.01
4171627-17162743.86345.27
5183519-18351946.90348.27
6178630-17863045.65347.04
点击查看处理图标(自动生成)
　
原始图谱下载图谱(王丹 于 2024-05-21 16:34:42 完成)
生成报告数据部分(等待生成报告)
Current page cost:54 ms