替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522621726108260732606825988260910.32
213.452603725965260010.20
单位质量响应值RSD%判断
1929.811933.160.13数据可信
供试品溶液-ald批-pH2.0盐酸溶液
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126838-2683897.47899.001.9797.4899.001.97
226572-2657296.51296.51
327769-27769100.860100.86
427035-2703598.19498.19
527938-27938101.474101.47
627397-2739799.50999.51
10min127125-2712598.521100.712.5699.50101.702.55
226679-2667996.90197.87
327783-27783100.911101.92
427984-27984101.641102.62
528210-28210102.461103.48
628591-28591103.845104.84
15min127620-27620100.319100.472.22102.28102.472.21
226752-2675297.16699.10
327458-2745899.730101.75
427462-2746299.745101.74
528497-28497103.504105.54
628185-28185102.371104.40
20min127298-2729899.14999.442.88102.11102.442.86
226003-2600394.44597.35
327369-2736999.407102.42
427380-2738099.447102.44
528367-28367103.032106.11
627849-27849101.150104.21
30min127284-2728499.09899.911.37103.05103.901.40
227057-2705798.274102.12
327729-27729100.714104.72
427291-2729199.124103.11
528104-28104102.076106.18
627577-27577100.162104.23
极限127156-2715698.63399.242.33103.58104.242.31
226227-2622795.259100.09
327646-27646100.413105.43
427131-2713198.542103.52
527836-27836101.103106.23
627944-27944101.495106.57
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522607126054260912613126043260780.14
213.452599726061260290.18
单位质量响应值RSD%判断
1928.851935.240.24数据可信
供试品溶液-ald批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125661-2566193.17694.902.3493.1894.902.34
226463-2646396.08896.09
326439-2643996.00196.00
426877-2687797.59297.59
525194-2519491.48191.48
626172-2617295.03295.03
10min126836-2683697.44398.391.2698.3799.341.27
227060-2706098.25699.22
327500-2750099.854100.81
427305-2730599.146100.12
526581-2658196.51797.43
627300-2730099.128100.08
15min127038-2703898.17699.191.07100.08101.121.07
227574-27574100.123102.07
327648-27648100.391102.35
427499-2749999.850101.82
527171-2717198.659100.54
626974-2697497.94499.89
20min126655-2665596.78698.511.8799.67101.441.84
227054-2705498.234101.18
327431-2743199.603102.57
427231-2723198.877101.84
526521-2652196.29999.17
627891-27891101.274104.19
30min126606-2660696.60898.621.30100.46102.531.30
227342-2734299.280103.21
327242-2724298.917102.88
427364-2736499.360103.31
526867-2686797.555101.38
627544-27544100.014103.95
极限126303-2630395.50897.141.95100.33102.041.92
226607-2660796.611101.53
327092-2709298.372103.32
427176-2717698.677103.63
526026-2602694.50299.31
627308-2730899.157104.09
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522591725913258382591925860258890.15
213.452621626171261940.13
单位质量响应值RSD%判断
1914.871947.511.20数据可信
供试品溶液-ald批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125778-2577893.64998.272.8693.6598.272.86
227118-2711898.51798.52
326485-2648596.21896.22
427656-27656100.472100.47
527713-27713100.679100.68
627542-27542100.058100.06
10min126589-2658996.595100.152.9097.53101.142.90
227940-27940101.503102.49
326759-2675997.21398.18
427339-2733999.320100.32
528519-28519103.607104.61
628263-28263102.677103.68
15min126538-2653896.410100.182.4798.31102.162.47
227386-2738699.491101.49
327385-2738599.487101.42
427494-2749499.883101.88
528179-28179102.372104.41
628469-28469103.425105.45
20min126516-2651696.330100.782.6499.20103.772.64
228055-28055101.921104.92
327200-2720098.815101.74
428053-28053101.914104.91
528193-28193102.423105.49
628436-28436103.305106.37
30min126218-2621895.24899.872.8199.08103.862.80
227453-2745399.734103.75
327154-2715498.648102.57
427615-27615100.323104.34
528050-28050101.903105.99
628449-28449103.353107.45
极限126662-2666296.86199.882.41101.64104.872.41
227635-27635100.395105.41
326712-2671297.042101.95
427832-27832101.111106.13
527820-27820101.068106.18
628298-28298102.804107.93
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522651726508265032646926380264750.22
213.452633126384263580.15
单位质量响应值RSD%判断
1958.211959.700.06数据可信
供试品溶液-ald批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125576-2557691.59295.052.1791.5995.052.17
227063-2706396.91796.92
326722-2672295.69695.70
426347-2634794.35394.35
526401-2640194.54694.55
627134-2713497.17197.17
10min126217-2621793.88796.571.6994.8097.521.70
227626-2762698.93399.90
326913-2691396.38097.34
426902-2690296.34097.28
526990-2699096.65597.60
627147-2714797.21898.19
15min126967-2696796.57398.081.2498.43100.001.24
227453-2745398.314100.27
327342-2734297.91699.84
427104-2710497.06498.97
527537-2753798.614100.53
627919-2791999.982101.93
20min128189-28189100.94998.561.88103.77101.451.82
227232-2723297.522100.46
327039-2703996.83199.73
427000-2700096.69199.57
527607-2760798.865101.76
628059-28059100.484103.43
30min126414-2641494.59396.881.6498.42100.761.62
227488-2748898.439102.36
326696-2669695.60399.47
426948-2694896.505100.35
527285-2728597.712101.60
627484-2748498.425102.37
极限126345-2634594.34696.592.5099.12101.442.43
227477-2747798.399103.30
326416-2641694.60099.42
426328-2632894.28599.09
527749-2774999.374104.24
627514-2751498.532103.46
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