替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572641726532262582644426263263830.46
213.652620026403263020.55
单位质量响应值RSD%判断
1944.221926.890.64数据可信
供试品溶液-1批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127373-2737399.21498.343.0999.2198.343.09
226303-2630395.33695.34
327965-27965101.360101.36
426843-2684397.29397.29
526156-2615694.80394.80
628147-28147102.020102.02
10min127438-2743899.45099.182.68100.44100.162.68
226268-2626895.20996.16
327551-2755199.860100.87
427774-27774100.668101.64
526806-2680697.15998.11
628343-28343102.730103.75
15min126578-2657896.33397.452.1898.3299.422.19
226373-2637395.59097.50
327331-2733199.062101.07
426865-2686597.37399.35
526351-2635195.51097.43
627819-27819100.831102.88
20min127131-2713198.33796.502.50101.2999.452.50
225725-2572593.24196.10
326786-2678697.087100.09
426606-2660696.43499.39
526012-2601294.28197.16
627489-2748999.635102.69
30min125437-2543792.19795.322.2996.1399.242.26
226017-2601794.30098.09
326435-2643595.81599.79
426755-2675596.974100.89
526027-2602794.33698.15
627124-2712498.312102.36
极限126139-2613994.74296.102.6699.60100.972.64
225819-2581993.58298.32
326735-2673596.902101.83
427006-2700697.884102.77
525826-2582693.60798.37
627561-2756199.896104.93
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572610826366262292615026344262390.44
213.652627926575264270.80
单位质量响应值RSD%判断
1933.601936.040.09数据可信
供试品溶液-1批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125782-2578293.48193.891.7093.4893.891.70
226015-2601594.32694.33
326098-2609894.62794.63
425687-2568793.13793.14
526546-2654696.25196.25
625243-2524391.52791.53
10min126186-2618694.94695.851.1095.8896.791.10
226619-2661996.51697.46
326281-2628195.29096.24
426491-2649196.05296.98
526894-2689497.51398.48
626141-2614194.78395.70
15min126133-2613394.75495.821.0196.6497.721.01
226618-2661896.51298.42
326589-2658996.40798.31
426416-2641695.78097.67
526718-2671896.87598.81
626083-2608394.57296.44
20min126302-2630295.36695.291.4498.2098.141.43
226538-2653896.22299.10
326454-2645495.91898.78
425943-2594394.06596.91
526718-2671896.87599.78
625724-2572493.27196.08
30min126488-2648896.04195.211.4499.8399.021.42
226270-2627095.25099.09
326075-2607594.54398.37
426136-2613694.76598.55
526840-2684097.317101.19
625743-2574393.34097.08
极限125677-2567793.10093.482.3097.8598.242.24
226245-2624595.16099.95
326096-2609694.62099.39
424980-2498090.57395.31
526469-2646995.972100.82
625227-2522791.46996.14
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572647326042262912622226215262490.60
213.652638726329263580.16
单位质量响应值RSD%判断
1934.341930.990.13数据可信
供试品溶液-1批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127015-2701598.06197.861.2598.0697.861.25
226483-2648396.13096.13
326854-2685497.47797.48
427180-2718098.66098.66
527446-2744699.62699.63
626774-2677497.18697.19
10min127847-27847101.081100.881.12102.06101.861.11
227564-27564100.054101.02
328080-28080101.927102.90
428209-28209102.395103.38
527399-2739999.455100.45
627658-27658100.395101.37
15min127553-27553100.01499.480.84102.01101.470.84
227020-2702098.079100.04
327457-2745799.666101.66
427679-27679100.471102.48
527438-2743899.597101.59
627292-2729299.067101.04
20min127257-2725798.94099.381.02101.93102.361.01
227154-2715498.566101.51
327503-2750399.833102.82
427861-27861101.132104.15
527107-2710798.395101.38
627384-2738499.401102.37
30min126710-2671096.95497.571.46100.93101.541.43
226218-2621895.16899.10
327004-2700498.021102.01
427375-2737599.368103.39
526899-2689997.640101.61
627072-2707298.268102.23
极限126374-2637495.73495.182.29100.68100.132.19
226374-2637495.734100.61
327016-2701698.065103.03
426534-2653496.315101.34
525606-2560692.94797.89
625419-2541992.26897.21
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572630325874260062628026030260990.72
213.652614326270262060.35
单位质量响应值RSD%判断
1923.291919.850.13数据可信
供试品溶液-1批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125433-2543392.85295.662.5292.8595.662.52
226308-2630896.04696.05
327013-2701398.62098.62
426577-2657797.02897.03
526506-2650696.76996.77
625379-2537992.65592.65
10min126162-2616295.51397.892.1696.4498.842.16
226788-2678897.79998.76
326889-2688998.16799.15
427589-27589100.723101.69
527285-2728599.613100.58
626165-2616595.52496.45
15min126307-2630796.04398.832.3797.93100.762.37
226979-2697998.496100.43
327281-2728199.598101.57
427963-27963102.088104.07
527487-27487100.351102.31
626404-2640496.39798.28
20min126025-2602595.01397.222.2397.86100.152.23
226536-2653696.87999.80
326934-2693498.332101.30
427414-27414100.084103.08
526986-2698698.521101.49
625887-2588794.50997.35
30min125730-2573093.93695.592.0797.7399.482.07
226018-2601894.98798.88
326343-2634396.174100.12
427013-2701398.620102.62
526465-2646596.619100.57
625523-2552393.18096.97
极限124774-2477490.44694.502.7295.1899.352.67
225705-2570593.84598.69
326136-2613695.418100.33
426373-2637396.283101.27
526768-2676897.726102.64
625548-2554893.27297.99
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