替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572665326355263432628226303263870.58
213.652641726381263990.10
单位质量响应值RSD%判断
1944.511933.990.39数据可信
供试品溶液批-pH6.8磷酸盐溶液
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122153-2215380.14078.903.0980.1478.903.09
222446-2244681.20081.20
320873-2087375.51075.51
421673-2167378.40478.40
522501-2250181.39981.40
621207-2120776.71876.72
10min124550-2455088.81188.772.0489.6189.562.04
225054-2505490.63591.45
323779-2377986.02286.78
424582-2458288.92789.71
525072-2507290.70091.51
624201-2420187.54988.32
15min125691-2569192.93991.852.2794.6393.522.28
226112-2611294.46296.18
324596-2459688.97890.59
424994-2499490.41892.09
525824-2582493.42095.14
625122-2512290.88192.52
20min125259-2525991.37691.612.2894.0094.212.27
226025-2602594.14796.81
324274-2427487.81390.32
425444-2544492.04694.62
525483-2548392.18794.84
625462-2546292.11194.66
30min125535-2553592.37593.821.4095.9197.341.40
226507-2650795.89199.50
325613-2561392.65796.04
425830-2583093.44296.94
525959-2595993.90997.49
626166-2616694.65798.13
极限125651-2565192.79494.142.6097.2598.592.56
227079-2707997.960102.52
325058-2505890.64994.96
425909-2590993.72898.16
526183-2618394.71999.24
626258-2625894.99099.41
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572641926309262512627926270263060.26
213.652750727472274900.10
单位质量响应值RSD%判断
1938.542013.922.70数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121302-2130275.64774.773.1875.6574.773.18
221345-2134575.79975.80
320388-2038872.40172.40
420707-2070773.53473.53
522133-2213378.59878.60
620457-2045772.64672.65
10min124323-2432386.37585.872.0587.1386.622.03
224843-2484388.22188.98
324236-2423686.06686.79
424454-2445486.84087.58
523459-2345983.30684.09
623771-2377184.41485.14
15min125433-2543390.31690.082.3691.9491.692.34
225842-2584291.76993.41
325151-2515189.31590.90
424920-2492088.49590.10
526231-2623193.15094.77
624619-2461987.42689.00
20min125330-2533089.95189.912.0392.4792.422.02
225600-2560090.90993.47
325005-2500588.79691.27
425317-2531789.90492.39
526085-2608592.63295.18
624578-2457887.28089.72
30min126014-2601492.38092.091.1895.8095.491.16
225728-2572891.36494.83
326311-2631193.43496.80
425680-2568091.19394.58
526252-2625293.22596.70
625605-2560590.92794.24
极限125483-2548390.49492.671.2894.8497.001.24
226206-2620693.06197.44
326174-2617492.94897.25
426212-2621293.08397.38
526475-2647594.01798.43
626028-2602892.42996.66
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.572609426066260012604626001260420.16
213.652595525940259480.05
单位质量响应值RSD%判断
1919.091900.950.68数据可信
供试品溶液批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min120796-2079676.38478.313.0676.3878.303.06
221847-2184780.24480.24
322176-2217681.45281.45
420806-2080676.42076.42
520639-2063975.80775.81
621651-2165179.52479.52
10min124601-2460190.35991.101.9291.1291.881.92
225582-2558293.96394.76
325156-2515692.39893.21
424658-2465890.56991.33
524295-2429589.23589.99
624527-2452790.08890.88
15min125544-2554493.82393.831.6095.4995.521.61
226171-2617196.12697.87
325778-2577894.68296.42
425524-2552493.74995.42
524990-2499091.78893.44
625265-2526592.79894.49
20min124991-2499191.79293.782.3594.4096.412.34
226387-2638796.91999.62
326081-2608195.79598.48
425449-2544993.47496.08
524857-2485791.30093.87
625423-2542393.37996.00
30min125757-2575794.60596.492.0698.13100.062.05
226770-2677098.326102.00
326757-2675798.278101.92
426237-2623796.36899.91
525496-2549693.64797.13
626599-2659997.698101.26
极限126096-2609695.85096.242.35100.32100.772.32
227252-27252100.096104.75
326277-2627796.515101.14
426211-2621196.273100.78
525348-2534893.10397.52
626023-2602395.582100.12
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