替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522578425576257952559325643256780.41
213.452587025899258840.08
单位质量响应值RSD%判断
1899.261924.460.94数据可信
供试品溶液-ald批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19713-971335.64238.064.9135.6438.064.91
210828-1082839.73439.73
310200-1020037.42937.43
411041-1104140.51540.52
59971-997136.58936.59
610484-1048438.47138.47
10min119531-1953171.67072.286.3272.0372.666.30
221033-2103377.18177.58
319824-1982472.74573.12
419300-1930070.82271.23
517612-1761264.62864.99
620881-2088176.62477.01
15min122884-2288483.97483.174.4685.0584.274.46
222869-2286983.91985.09
322932-2293284.15085.25
422709-2270983.33184.44
520771-2077176.22077.23
623823-2382387.41988.57
20min122768-2276883.54884.822.8485.4686.762.87
223392-2339285.83887.85
323468-2346886.11788.06
423550-2355086.41788.36
521924-2192480.45182.23
623587-2358786.55388.58
30min124135-2413588.56486.545.7991.3189.335.71
224405-2440589.55592.42
323985-2398588.01490.82
422604-2260482.94685.76
521333-2133378.28280.86
625044-2504491.90094.79
极限123047-2304784.57284.315.2188.2187.965.12
222009-2200980.76384.53
323606-2360686.62390.31
423161-2316184.99088.63
521315-2131578.21681.58
624712-2471290.68194.49
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522584125705259022569025712257700.38
213.452574925857258030.30
单位质量响应值RSD%判断
1906.071918.440.46数据可信
供试品溶液-ald批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19238-923833.89137.485.7133.8937.485.71
210091-1009137.02037.02
310327-1032737.88637.89
410044-1004436.84836.85
510822-1082239.70239.70
610777-1077739.53739.54
10min118131-1813166.51672.625.3466.8673.005.34
220219-2021974.17774.55
319285-1928570.75071.13
419519-1951971.60971.98
520465-2046575.07975.48
621153-2115377.60378.00
15min122933-2293384.13382.803.0485.1483.903.01
223338-2333885.61986.73
321506-2150678.89879.98
422011-2201180.75181.84
522646-2264683.08084.23
622987-2298784.33285.50
20min121451-2145178.69684.794.1380.5486.724.11
223487-2348786.16688.13
322744-2274483.44085.32
423335-2333585.60887.50
523363-2336385.71187.69
624298-2429889.14191.16
30min122068-2206880.96086.953.6583.5989.723.63
224476-2447689.79492.62
323581-2358186.51189.22
423862-2386287.54290.29
523891-2389187.64890.48
624324-2432489.23792.14
极限121433-2143378.63084.204.9982.0787.854.93
223384-2338485.78889.52
321834-2183480.10283.68
422922-2292284.09387.72
523674-2367486.85290.56
624464-2446489.75093.55
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522590425874257682572225747258030.32
213.452583025991259100.44
单位质量响应值RSD%判断
1908.511926.390.66数据可信
供试品溶液-ald批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min113965-1396551.09550.153.2151.0950.163.21
214148-1414851.76451.76
313682-1368250.05950.06
413859-1385950.70750.71
512881-1288147.12847.13
613714-1371450.17650.18
10min122132-2213280.97679.062.5181.4979.562.52
221944-2194480.28880.81
321920-2192080.20080.70
421719-2171979.46579.97
520698-2069875.72976.20
621231-2123177.67978.18
15min123666-2366686.58885.041.4087.9186.341.38
223101-2310184.52185.84
323312-2331285.29386.60
422703-2270383.06584.37
523268-2326885.13286.36
623411-2341185.65586.93
20min124814-2481490.78888.692.2692.9790.842.23
224725-2472590.46392.63
323961-2396187.66789.82
423447-2344785.78787.92
523918-2391887.51089.59
624586-2458689.95492.09
30min125495-2549593.28089.452.5196.3792.482.47
224794-2479490.71593.79
324054-2405488.00891.04
424349-2434989.08792.08
523788-2378887.03589.99
624216-2421688.60091.64
极限124935-2493591.23188.292.4795.2692.212.44
224310-2431088.94492.92
324249-2424988.72192.63
423959-2395987.66091.54
523109-2310984.55088.38
624222-2422288.62292.54
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.522564825680255512545025654255970.38
213.452585525833258440.07
单位质量响应值RSD%判断
1893.271921.491.05数据可信
供试品溶液-ald批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min113620-1362050.09749.552.1850.1049.552.18
213328-1332849.02349.02
312967-1296747.69547.70
413454-1345449.48649.49
513708-1370850.42150.42
613746-1374650.56150.56
10min120679-2067976.06177.841.8376.5678.331.82
220762-2076276.36776.86
321077-2107777.52578.00
421423-2142378.79879.29
521638-2163879.58980.09
621389-2138978.67379.18
15min122430-2243082.50283.842.2783.7685.122.26
222358-2235882.23783.49
322273-2227381.92483.18
423006-2300684.62185.90
523547-2354786.61187.91
623155-2315585.16986.46
20min122811-2281183.90387.302.2885.9989.412.23
224144-2414488.80690.88
323985-2398588.22290.29
423343-2334385.86087.99
524081-2408188.57590.74
624043-2404388.43590.58
30min122553-2255382.95488.253.4285.8891.233.34
223660-2366087.02689.99
324572-2457290.38193.33
423910-2391087.94690.93
524564-2456490.35193.40
624696-2469690.83793.87
极限123384-2338486.01187.681.5389.7791.551.52
223763-2376387.40591.24
324223-2422389.09792.95
423446-2344686.23990.11
524138-2413888.78492.74
624072-2407288.54292.48
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