氢溴酸氟硫西汀口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号D382/2305001对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.83对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.7867
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.718794287959879298795487882879330.04
213.768791687857878860.05
单位质量响应值RSD%判断
6413.796387.060.30数据可信
供试品溶液-2024051221批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min160787-6078767.13066.235.1567.1366.235.15
261572-6157267.99768.00
362305-6230568.80668.81
460374-6037466.67466.67
560959-6095967.32067.32
653826-5382659.44359.44
5min185322-8532294.22593.772.2994.2393.772.29
286928-8692895.99996.00
386590-8659095.62595.63
485050-8505093.92593.92
581616-8161690.13290.13
683962-8396292.72392.72
10min189067-8906798.36197.502.4198.3697.502.41
290175-9017599.58599.58
390111-9011199.51499.51
488154-8815497.35397.35
584461-8446193.27493.27
687747-8774796.90396.90
15min189560-8956098.90598.292.0398.9198.292.03
290404-9040499.83799.84
391049-91049100.550100.55
488824-8882498.09398.09
585997-8599794.97194.97
688170-8817097.37097.37
20min190175-9017599.58598.342.5799.5898.342.57
290914-90914100.401100.40
391019-91019100.517100.52
488631-8863197.87997.88
584907-8490793.76793.77
688637-8863797.88697.89
30min190278-9027899.69898.362.5099.7098.362.50
291066-91066100.569100.57
390830-90830100.308100.31
488789-8878998.05498.05
585140-8514094.02494.02
688311-8831197.52697.53
45min190834-90834100.31298.402.61100.3198.402.61
290822-90822100.299100.30
390762-90762100.233100.23
489006-8900698.29498.29
584897-8489793.75693.76
688305-8830597.51997.52
60min190923-90923100.41198.492.71100.4198.492.71
291150-91150100.661100.66
390747-90747100.216100.22
488715-8871597.97297.97
584786-8478693.63393.63
688777-8877798.04198.04
极限191297-91297100.82498.462.62100.8298.462.62
290825-90825100.302100.30
390632-90632100.089100.09
488713-8871397.97097.97
585052-8505293.92793.93
688409-8840997.63497.63
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