托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号TAAF230001对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数10000
标示量(mg)15供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.981015771015141014021012571012301013960.16
217.091034471035611035040.08
单位质量响应值RSD%判断
5971.506056.411.00数据可信
供试品溶液-24051301批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17166-71667.1357.493.047.147.503.02
27653-76537.6207.62
37554-75547.5227.52
47852-78527.8197.82
57452-74527.4207.42
67478-74787.4467.45
10min117132-1713217.05917.632.3417.1017.682.33
217520-1752017.44517.49
317403-1740317.32917.37
418061-1806117.98418.03
517991-1799117.91417.96
618141-1814118.06418.10
15min123175-2317523.07623.501.8223.2123.641.82
223342-2334223.24223.38
323311-2331123.21223.35
424261-2426124.15824.30
523981-2398123.87924.02
623520-2352023.42023.56
20min127477-2747727.36027.801.5227.6228.071.52
227546-2754627.42827.70
327813-2781327.69427.96
428637-2863728.51528.79
527970-2797027.85128.12
628099-2809927.97928.25
30min132992-3299232.85132.971.5233.2733.401.50
232555-3255532.41632.84
332976-3297632.83533.26
433830-3383033.68634.12
533600-3360033.45733.88
632720-3272032.58033.01
45min138226-3822638.06338.702.0338.6639.312.03
237911-3791137.74938.35
338464-3846438.30038.90
439809-3980939.63940.26
539691-3969139.52240.14
639101-3910138.93439.54
60min142149-4214941.96942.622.1342.7843.442.11
242229-4222942.04942.86
341811-4181141.63342.45
443892-4389243.70544.55
543898-4389843.71144.54
642828-4282842.64543.47
90min148672-4867248.46448.401.1849.5149.461.18
248260-4826048.05449.10
347670-4767047.46748.51
449095-4909548.88649.97
548717-4871748.50949.59
649223-4922349.01350.07
120min153106-5310652.87953.031.9654.1954.361.94
252781-5278152.55653.87
351959-5195951.73753.05
455114-5511454.87956.24
553228-5322853.00154.35
653370-5337053.14254.48
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限157292-5729257.04857.481.5558.6559.101.54
258031-5803157.78359.39
356463-5646356.22257.82
458723-5872358.47360.14
557202-5720256.95858.60
658639-5863958.38960.02
托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号TAAF230001对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数10000
标示量(mg)15供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.981025031024521022371021401021221022910.18
217.091050041050951050500.07
单位质量响应值RSD%判断
6024.206146.871.43数据可信
供试品溶液-24051302批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min18037-80377.9097.716.157.917.716.16
27198-71987.0837.08
37298-72987.1827.18
48419-84198.2858.28
58094-80947.9657.97
67961-79617.8347.83
10min119404-1940419.09518.893.5319.1418.933.55
218104-1810417.81617.85
318699-1869918.40118.44
419832-1983219.51619.56
519827-1982719.51119.56
619290-1929018.98319.03
15min126045-2604525.63025.403.1625.7825.543.17
225164-2516424.76324.90
324477-2447724.08724.23
426342-2634225.92226.08
526589-2658926.16526.32
626227-2622725.80925.96
20min131339-3133930.84030.192.3631.1330.482.34
231191-3119130.69430.97
329551-2955129.08029.36
430789-3078930.29930.60
531139-3113930.64330.94
630037-3003729.55929.85
30min137173-3717336.58136.822.3237.0437.282.31
236075-3607535.50035.95
336978-3697836.38936.83
437748-3774837.14737.61
537948-3794837.34437.81
638565-3856537.95138.41
45min143335-4333542.64542.411.9143.3143.071.91
242189-4218941.51742.16
342363-4236341.68842.33
444463-4446343.75544.43
543289-4328942.60043.28
642917-4291742.23342.90
60min147791-4779147.03047.611.9447.9348.511.93
248161-4816147.39448.27
347557-4755746.80047.67
448822-4882248.04448.96
550077-5007749.27950.19
647891-4789147.12848.03
90min155050-5505054.17353.881.3255.3455.041.32
254189-5418953.32654.46
353721-5372152.86554.00
454957-5495754.08255.26
554790-5479053.91755.10
655794-5579454.90556.07
120min159282-5928258.33859.361.3759.8060.821.36
260191-6019159.23260.67
359507-5950758.55959.98
461196-6119660.22161.70
560568-6056859.60361.09
661208-6120860.23361.70
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限164885-6488563.85263.331.7965.6465.121.78
262812-6281261.81263.57
363667-6366762.65364.40
465366-6536664.32566.14
565749-6574964.70266.52
663629-6362962.61664.42
点击查看处理图标(自动生成)
　
原始图谱下载图谱(王丹 于 2024-05-28 19:44:46 完成)
生成报告数据部分(等待生成报告)
Current page cost:36 ms