叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.909605796314961309611096197961620.11
210.099837398202982880.13
单位质量响应值RSD%判断
9713.339741.130.21数据可信
供试品溶液-24052303批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111865-1186520.02428.0818.5220.0228.0818.52
218720-1872031.59331.59
317972-1797230.33030.33
415304-1530425.82825.83
520551-2055134.68334.68
615428-1542826.03726.04
10min124657-2465741.61249.259.4941.8349.569.55
230853-3085352.06952.42
330928-3092852.19552.53
428054-2805447.34547.63
532328-3232854.55854.94
628283-2828347.73148.02
15min125241-2524142.59858.0913.7543.2858.9513.72
236140-3614060.99161.92
337180-3718062.74663.66
434110-3411057.56558.38
538420-3842064.83965.83
635427-3542759.78860.61
20min128810-2881048.62166.6415.2249.7868.1415.14
241161-4116169.46571.07
339234-3923466.21367.83
440316-4031668.03969.49
547399-4739979.99281.70
640006-4000667.51669.00
30min129280-2928049.41473.9316.3051.1176.1816.18
246170-4617077.91880.30
347547-4754780.24282.59
446453-4645378.39680.60
547213-4721379.67882.28
646186-4618677.94580.18
45min132189-3218954.32381.0616.2756.5784.1316.16
250087-5008784.52987.77
352744-5274489.01392.25
450937-5093785.96389.04
551544-5154486.98890.47
650698-5069885.56088.66
60min133645-3364556.78183.8916.0059.6387.8615.90
252044-5204487.83192.02
354174-5417491.42695.66
453753-5375390.71694.75
553462-5346290.22494.68
651158-5115886.33690.39
90min130214-3021450.99087.0020.4554.4791.9020.11
253899-5389990.96296.12
358048-5804897.964103.21
456009-5600994.52399.57
555847-5584794.24999.70
655290-5529093.30998.32
极限139398-3939866.49091.4813.5270.5497.3513.63
256912-5691296.047102.22
358398-5839898.555104.89
456484-5648495.324101.42
558254-5825498.312104.81
655787-5578794.148100.20
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