叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.091234649123585812339051235652123453512349200.07
29.901223633122231912229760.08
单位质量响应值RSD%判断
122390.49123532.930.66数据可信
供试品溶液-22FA458批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19581-95811.2791.5938.391.281.5938.35
212376-123761.6521.65
310484-104841.4001.40
410026-100261.3391.34
520747-207472.7702.77
68072-80721.0781.08
10min135872-358724.7895.1936.804.805.2036.82
243155-431555.7625.78
330748-307484.1054.12
431635-316354.2244.24
565575-655758.7558.79
626101-261013.4853.50
15min166027-660278.8159.6726.218.889.7526.28
275742-7574210.11210.19
375216-7521610.04210.10
462001-620018.2788.34
5105901-10590114.13914.27
649773-497736.6456.70
20min195252-9525212.71713.7320.9612.8813.9121.06
2105584-10558414.09614.29
3112901-11290115.07315.25
489056-8905611.89012.04
5138188-13818818.44918.73
676070-7607010.15610.28
30min1142697-14269719.05120.4815.4019.3620.8215.55
2157834-15783421.07221.42
3162544-16254421.70122.04
4135007-13500718.02418.31
5193719-19371925.86326.35
6128764-12876417.19117.43
45min1196756-19675626.26829.2914.2126.7929.8514.30
2215588-21558828.78329.37
3248536-24853633.18233.76
4194374-19437425.95026.44
5266524-26652435.58336.36
6194333-19433325.94526.37
60min1233372-23337231.15735.4812.9331.9736.3713.01
2256235-25623534.20935.11
3304056-30405640.59441.54
4240066-24006632.05132.83
5313687-31368741.88043.05
6247305-24730533.01733.73
90min1288838-28883838.56244.0811.5139.7245.3611.55
2309640-30964041.33942.62
3379825-37982550.71052.11
4304827-30482740.69741.83
5374103-37410349.94651.58
6323773-32377343.22644.31
极限1334210-33421044.62049.339.2946.2051.119.44
2351976-35197646.99248.74
3408610-40861054.55356.52
4348352-34835246.50848.09
5416546-41654655.61257.81
6357388-35738847.71449.28
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.091222873122226712224401222159122193012223340.03
29.901207946120526812066070.16
单位质量响应值RSD%判断
121143.11121879.490.43数据可信
供试品溶液-22FA458批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13161-31610.4270.5121.490.430.5221.83
24481-44810.6050.61
33115-31150.4210.42
43217-32170.4350.43
53772-37720.5100.51
65091-50910.6880.69
10min1-0.0000.7451.000.000.7451.05
27845-78451.0601.07
36093-60930.8230.83
45543-55430.7490.75
56795-67950.9180.92
66441-64410.8700.88
15min14051-40510.5471.2432.430.551.2632.49
212992-129921.7551.77
310534-105341.4231.44
48221-82211.1111.12
510185-101851.3761.39
69285-92851.2541.27
20min15767-57670.7791.8635.430.791.8935.31
220607-206072.7842.82
316377-163772.2132.24
412733-127331.7201.75
513930-139301.8821.91
613223-132231.7861.82
30min19379-93791.2673.1736.161.293.2236.07
235598-355984.8094.88
327132-271323.6663.72
422882-228823.0913.14
522429-224293.0303.08
623504-235043.1753.23
45min118054-180542.4395.4232.352.475.5032.39
257804-578047.8097.93
346373-463736.2656.36
438768-387685.2385.32
539840-398405.3825.47
639733-397335.3685.45
60min128379-283793.8347.6428.223.897.7828.33
276490-7649010.33410.54
364876-648768.7658.93
453778-537787.2657.40
557507-575077.7697.91
658182-581827.8608.01
90min148249-482496.51811.3523.316.6211.5823.46
2103710-10371014.01114.34
393000-9300012.56412.83
481433-8143311.00211.22
581271-8127110.98011.21
696414-9641413.02613.26
极限165752-657528.88313.6718.369.0614.0318.59
2118503-11850316.01016.49
3111834-11183415.10915.51
499732-9973213.47413.81
5108258-10825814.62614.98
6103188-10318813.94114.32
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.091209850120799712094191207614120689512083550.11
29.901194778119304411939110.11
单位质量响应值RSD%判断
119757.68120597.070.50数据可信
供试品溶液-22FA458批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17314-73140.9991.0015.131.001.0115.18
27453-74531.0181.02
37332-73321.0021.00
45405-54050.7380.74
57799-77991.0651.07
68832-88321.2061.21
10min19678-96781.3221.5431.771.331.5531.46
213182-131821.8011.81
39341-93411.2761.29
47379-73791.0081.02
510649-106491.4551.47
617501-175012.3912.40
15min114805-148052.0222.4739.462.052.5039.20
223706-237063.2383.27
313925-139251.9021.93
410400-104001.4211.44
516170-161702.2092.24
629603-296034.0444.08
20min121033-210332.8733.5443.732.923.6043.56
230266-302664.1344.20
322259-222593.0413.09
413744-137441.8771.91
521771-217712.9743.03
646417-464176.3416.43
30min141476-414765.6666.9155.155.757.0154.86
257609-576097.8697.98
340521-405215.5355.62
422058-220583.0133.07
539179-391795.3525.44
6102682-10268214.02614.18
45min184333-8433311.52012.9252.3111.6613.0952.20
298874-9887413.50613.71
381131-8113111.08211.22
441005-410055.6015.69
574525-7452510.18010.33
6187638-18763825.63125.94
60min1135057-13505718.44919.2945.7418.7219.6045.77
2141965-14196519.39219.74
3128620-12862017.56917.83
471815-718159.8109.96
5107391-10739114.67014.93
6262465-26246535.85336.45
90min1228902-22890231.26830.3538.1831.7430.8838.32
2209811-20981128.66029.23
3211849-21184928.93929.40
4133683-13368318.26118.52
5168547-16854723.02323.44
6380164-38016451.93052.92
极限1310557-31055742.42241.3823.8543.2542.2424.24
2295653-29565340.38641.27
3300651-30065141.06941.85
4226280-22628030.91031.37
5249867-24986734.13234.81
6434382-43438259.33660.91
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