贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.88 3000182995702997493000752998432998510.07
29.922985772995532990650.24
单位质量响应值RSD%判断
30349.2930147.680.48数据可信
供试品溶液-24051501SP批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19635-96356.3535.539.516.355.539.46
27566-75664.9894.99
37501-75014.9464.95
48588-85885.6625.66
58727-87275.7545.75
68306-83065.4775.48
10min125396-2539616.74515.695.1016.8215.765.10
224998-2499816.48216.54
323134-2313415.25315.31
422125-2212514.58814.65
523700-2370015.62715.69
623460-2346015.46815.53
15min139117-3911725.79224.214.4426.0524.454.45
237251-3725124.56124.80
336233-3623323.89024.11
435008-3500823.08223.31
537744-3774424.88625.12
634976-3497623.06123.29
20min148231-4823131.80129.963.1532.3430.473.16
245581-4558130.05430.57
345073-4507329.71930.21
444519-4451929.35329.83
544857-4485729.57630.09
644414-4441429.28429.77
30min159167-5916739.01237.822.2739.9138.662.28
256139-5613937.01537.86
357057-5705737.62038.44
457467-5746737.89138.70
558474-5847438.55539.40
655839-5583936.81737.63
45min174231-7423148.94446.333.6750.2747.593.65
269642-6964245.91847.17
370784-7078446.67147.91
467803-6780344.70645.93
571777-7177747.32648.60
667369-6736944.41945.64
60min183410-8341054.99651.124.3556.8752.904.31
276389-7638950.36752.13
376873-7687350.68652.44
475420-7542049.72851.45
579234-7923452.24354.04
673906-7390648.73050.45
极限191905-9190560.59758.042.5263.0860.382.55
285903-8590356.64058.97
387511-8751157.70060.02
487125-8712557.44659.72
589227-8922758.83161.21
686462-8646257.00859.27
贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.88 2987772983432986202981162984592984630.09
29.922985492991652988570.15
单位质量响应值RSD%判断
30208.8130126.710.20数据可信
供试品溶液-24052101SP批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min152624-5262434.79033.964.4634.7933.964.46
252004-5200434.38034.38
353778-5377835.55335.55
447522-4752231.41731.42
552486-5248634.69934.70
649816-4981632.93432.93
10min1110771-11077173.23164.206.9873.6264.586.96
295644-9564463.23163.61
394747-9474762.63863.03
493070-9307061.52961.88
595305-9530563.00763.39
693139-9313961.57561.94
15min1132375-13237587.51475.477.8688.7176.567.82
2110259-11025972.89373.98
3112152-11215274.14475.24
4109612-10961272.46573.50
5110772-11077273.23274.32
6109766-10976672.56773.62
20min1128492-12849284.94780.063.0387.1281.983.11
2119199-11919978.80380.70
3119591-11959179.06280.98
4118856-11885678.57680.41
5120150-12015079.43281.33
6120270-12027079.51181.37
30min1128901-12890185.21784.900.9788.3387.720.99
2127377-12737784.20986.98
3127618-12761884.36987.16
4127040-12704083.98786.70
5129626-12962685.69688.48
6129967-12996785.92288.66
45min1133820-13382088.46989.591.3492.5393.351.24
2135605-13560589.64993.35
3134189-13418988.71392.44
4134079-13407988.64092.28
5137725-13772591.05194.78
6137700-13770091.03494.73
60min1130480-13048086.26187.922.2891.3192.682.13
2131039-13103986.63091.33
3130361-13036186.18290.90
4132528-13252887.61592.24
5137181-13718190.69195.44
6136316-13631690.11994.83
极限1134981-13498189.23790.871.0895.2496.600.93
2137846-13784691.13196.79
3137767-13776791.07896.75
4136858-13685890.47796.08
5137721-13772191.04896.80
6139497-13949792.22297.93
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