氢溴酸氟硫西汀片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号D382/2305001对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.83对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.7867
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.001873111870731869601871281871061871160.07
214.011826721830151828440.14
单位质量响应值RSD%判断
13365.4313050.961.69数据可信
供试品溶液-2757904批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min121487-2148711.50012.266.5511.5012.266.55
224477-2447713.10113.10
322775-2277512.19012.19
5min1103440-10344055.36355.193.6955.3655.193.69
2106761-10676157.14057.14
399170-9917053.07853.08
10min1142358-14235876.19376.636.7776.1976.636.76
2153234-15323482.01482.01
3133922-13392271.67771.68
15min1165681-16568188.67584.628.1888.6884.628.18
2165454-16545488.55488.55
3143190-14319076.63876.64
20min1171829-17182991.96687.538.1491.9787.538.14
2170589-17058991.30291.30
3148194-14819479.31679.32
30min1172424-17242492.28489.017.4392.2889.017.43
2174405-17440593.34593.34
3152095-15209581.40481.40
45min1176610-17661094.52590.778.0394.5290.778.03
2178278-17827895.41895.42
3153912-15391282.37682.38
60min1177935-17793595.23492.156.3595.2392.156.36
2179021-17902195.81595.82
3159567-15956785.40385.40
极限1179219-17921995.92196.630.7195.9296.630.71
2181738-18173897.26997.27
3180691-18069196.70996.71
氢溴酸氟硫西汀片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号D382/2305001对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.83对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.7867
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.001830361830081830171829451829301829870.03
214.011835381833101834240.09
单位质量响应值RSD%判断
13070.5013092.360.12数据可信
供试品溶液-2757904批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min165298-6529835.28229.5227.6435.2829.5227.63
261241-6124133.09033.09
337360-3736020.18720.19
5min1100795-10079554.46259.068.9154.4659.068.91
2119926-11992664.79964.80
3107204-10720457.92557.93
10min1115392-11539262.35069.459.8462.3569.459.84
2140594-14059475.96775.97
3129630-12963070.04370.04
15min1121764-12176465.79374.0611.0665.7974.0611.07
2152074-15207482.17082.17
3137368-13736874.22474.22
20min1128047-12804769.18776.079.0469.1976.079.04
2153493-15349382.93782.94
3140806-14080676.08176.08
30min1133866-13386672.33280.429.5672.3380.439.56
2162156-16215687.61787.62
3150513-15051381.32681.33
45min1144178-14417877.90384.547.2577.9084.547.25
2166513-16651389.97289.97
3158683-15868385.74185.74
60min1150561-15056181.35288.056.7881.3588.056.78
2171755-17175592.80492.80
3166552-16655289.99389.99
极限1183773-18377399.29898.891.0299.3098.891.02
2184381-18438199.62699.63
3180907-18090797.74997.75
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