叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.141254852125356112534401253895125325112538000.06
210.181249519125000712497630.03
单位质量响应值RSD%判断
123648.92122766.500.51数据可信
供试品溶液-23FA408批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min169498-694989.2609.402.779.269.402.76
272896-728969.7139.71
371447-714479.5209.52
468136-681369.0789.08
572362-723629.6429.64
668971-689719.1909.19
10min1133754-13375417.82118.162.1717.9218.262.17
2137398-13739818.30718.41
3141303-14130318.82718.93
4133219-13321917.75017.85
5136867-13686718.23618.34
6135321-13532118.03018.13
15min1188956-18895625.17724.751.9125.4825.051.90
2185115-18511524.66524.98
3190758-19075825.41725.73
4181208-18120824.14424.44
5184752-18475224.61624.93
6183542-18354224.45524.76
20min1224139-22413929.86430.121.3730.4430.701.38
2224383-22438329.89730.48
3231834-23183430.89031.49
4223470-22347029.77530.34
5226808-22680830.22030.80
6225499-22549930.04630.62
30min1281223-28122337.47037.671.1338.3838.581.14
2283745-28374537.80638.72
3287842-28784238.35239.29
4278201-27820137.06837.96
5282040-28204037.57938.50
6283262-28326237.74238.65
45min1349434-34943446.55946.331.5647.8947.661.54
2344101-34410145.84847.19
3351122-35112246.78448.15
4338391-33839145.08746.40
5350504-35050446.70148.04
6352669-35266946.99048.32
60min1398425-39842553.08652.870.7654.9354.710.75
2392241-39224152.26254.11
3398215-39821553.05854.94
4395250-39525052.66354.47
5395739-39573952.72854.58
6400783-40078353.40055.25
90min1470906-47090662.74462.440.7965.1864.880.78
2469346-46934662.53664.96
3468689-46868962.44864.92
4461435-46143561.48263.88
5471444-47144462.81565.26
6469945-46994562.61665.06
极限1502060-50206066.89566.260.8970.0369.390.87
2493014-49301465.68968.81
3495319-49531965.99669.17
4491896-49189665.54068.62
5500834-50083466.73169.87
6500574-50057466.69769.84
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.141257664125707912580731259795125745912580140.09
210.181245062124597412455180.06
单位质量响应值RSD%判断
124064.50122349.510.99数据可信
供试品溶液-23FA408批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min173478-734789.79110.819.049.7910.809.06
280845-8084510.77210.77
381655-8165510.88010.88
479197-7919710.55310.55
594753-9475312.62512.63
676638-7663810.21210.21
10min1133173-13317317.74519.0410.2017.8519.1610.19
2136563-13656318.19618.32
3142118-14211818.93719.06
4140711-14071118.74918.87
5171624-17162422.86823.01
6133119-13311917.73817.85
15min1173070-17307023.06124.439.2723.3724.769.27
2176037-17603723.45623.78
3183217-18321724.41324.74
4183487-18348724.44924.77
5215866-21586628.76329.16
6168310-16831022.42722.74
20min1205864-20586427.43028.674.4927.9929.284.54
2206374-20637427.49828.08
3210788-21078828.08728.69
4215077-21507728.65829.26
5230176-23017630.67031.38
6222791-22279129.68630.25
30min1253176-25317633.73533.804.8234.6034.724.85
2249025-24902533.18134.07
3252078-25207833.58834.50
4259568-25956834.58635.50
5272512-27251236.31137.37
6235478-23547831.37632.27
45min1311243-31124341.47240.143.3742.7141.433.30
2302396-30239640.29341.55
3299036-29903639.84541.13
4310345-31034541.35242.65
5301065-30106540.11641.57
6283206-28320637.73638.97
60min1360418-36041848.02445.274.6549.7347.014.41
2347365-34736546.28547.99
3335280-33528044.67546.41
4350761-35076146.73748.50
5320634-32063442.72344.63
6323900-32390043.15844.82
90min1437699-43769958.32153.717.3760.5655.957.01
2415427-41542755.35457.57
3397092-39709252.91155.14
4420663-42066356.05258.33
5351445-35144546.82949.21
6396026-39602652.76954.91
极限1496761-49676166.19163.224.2569.0866.064.08
2482664-48266464.31367.15
3472571-47257162.96865.78
4486575-48657564.83467.74
5438524-43852458.43161.33
6469651-46965162.57965.30
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