叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.142520442521112524242524422516062521250.14
210.182503482501252502360.07
单位质量响应值RSD%判断
24864.4024581.140.82数据可信
供试品溶液-24052802批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min138651-3865125.66525.052.5925.6725.052.59
237447-3744724.86624.87
338986-3898625.88825.89
437879-3787925.15325.15
536914-3691424.51224.51
636484-3648424.22624.23
10min157491-5749138.17537.983.9038.4638.263.88
256378-5637837.43637.71
358478-5847838.83139.12
460647-6064740.27140.55
555953-5595337.15437.43
654203-5420335.99236.26
15min167907-6790745.09244.985.1945.8045.685.15
265756-6575643.66444.36
369270-6927045.99746.72
473780-7378048.99249.72
565888-6588843.75144.44
663819-6381942.37743.05
20min175249-7524949.96749.425.7451.1850.625.69
272959-7295948.44749.62
374784-7478449.65850.89
482061-8206154.49155.76
571914-7191447.75348.92
669579-6957946.20247.34
30min182685-8268554.90555.746.1056.6757.496.01
279417-7941752.73554.45
381957-8195754.42256.20
493458-9345862.05863.94
580526-8052653.47155.17
685591-8559156.83558.49
45min190023-9002359.77859.117.7362.1561.477.60
285942-8594257.06859.37
388566-8856658.81061.20
4101782-10178267.58670.15
586071-8607157.15359.45
681678-8167854.23656.52
60min193641-9364162.18060.808.7665.2263.838.58
287708-8770858.24061.18
389644-8964459.52662.57
4106500-10650070.71974.04
588436-8843658.72461.65
683486-8348655.43758.32
90min197723-9772364.89164.498.1668.6268.198.03
292394-9239461.35264.93
394354-9435462.65366.35
4112469-11246974.68278.79
595276-9527663.26666.85
690479-9047960.08063.58
极限1112428-11242874.65575.893.1079.1180.313.25
2113013-11301375.04379.31
3115572-11557276.74381.14
4120889-12088980.27385.21
5112532-11253274.72479.01
6111279-11127973.89278.06
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