贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.892976582979092979022979112979372978630.04
29.862983892989142986520.13
单位质量响应值RSD%判断
30117.5930289.250.41数据可信
供试品溶液-24060301批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min147520-4752015.68916.4017.7215.6916.4017.72
267087-6708722.15022.15
343676-4367614.42014.42
444711-4471114.76214.76
545328-4532814.96614.97
649729-4972916.41916.42
10min1132594-13259443.77844.618.7043.9544.798.73
2158291-15829152.26252.51
3125562-12556241.45641.62
4129043-12904342.60542.77
5134196-13419644.30744.47
6130947-13094743.23443.42
15min1187000-18700061.74162.273.6162.4062.953.65
2199247-19924765.78466.61
3189152-18915262.45163.07
4183652-18365260.63561.27
5192616-19261663.59564.25
6180010-18001059.43360.10
20min1213961-21396170.64270.972.7871.9972.342.81
2221599-22159973.16474.72
3215796-21579671.24872.56
4211830-21183069.93971.25
5220859-22085972.92074.28
6205616-20561667.88769.21
30min1246561-24656181.40680.962.0683.5483.122.08
2248710-24871082.11584.49
3245136-24513680.93583.04
4242150-24215079.94982.04
5251507-25150783.03985.21
6237248-23724878.33180.41
45min1272519-27251989.97689.331.3293.0192.391.37
2272560-27256089.98993.27
3269328-26932888.92291.93
4269024-26902488.82291.80
5275043-27504390.80993.91
6264910-26491087.46490.41
60min1285855-28585594.37993.710.8998.4197.760.93
2284413-28441393.90398.19
3282946-28294693.41997.41
4282448-28244893.25497.22
5287086-28708694.78598.89
6280145-28014592.49496.41
极限1291913-29191396.37996.380.43101.46101.480.47
2291514-29151496.247101.57
3293452-29345296.887101.92
4290859-29085996.031101.03
5293368-29336896.860102.02
6290480-29048095.906100.85
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