恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DC033-12306002对照品来源分装对照品使用方法直接使用
对照品含量(%)98.99对照品水分(%)0对照品稀释倍数400
标示量(mg)25供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.285624655622915622045624235621445623050.03
210.215627035630735628880.05
单位质量响应值RSD%判断
54698.9355131.050.56数据可信
供试品溶液-F56971批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1407803-40780366.16166.0112.9466.1666.0112.94
2443467-44346771.94771.95
3306903-30690349.79149.79
4407502-40750266.11266.11
5420503-42050368.22168.22
6455178-45517873.84773.85
10min1535126-53512686.81786.496.2486.9386.606.25
2540692-54069287.72087.84
3475365-47536577.12277.20
4532582-53258286.40486.51
5535607-53560786.89587.01
6579107-57910793.95394.08
15min1571549-57154992.72691.505.1292.9891.765.12
2558750-55875090.65090.92
3518096-51809684.05484.27
4561749-56174991.13691.39
5565606-56560691.76292.02
6608240-60824098.67998.96
20min1588558-58855895.48693.604.4295.9094.014.43
2564137-56413791.52491.94
3539328-53932887.49987.85
4574181-57418193.15393.56
5579542-57954294.02394.43
6615946-61594699.929100.37
30min1606146-60614698.33995.753.6398.9196.313.64
2568714-56871492.26692.84
3566507-56650791.90892.41
4588306-58830695.44596.01
5589408-58940895.62496.19
6621993-621993100.910101.52
45min1617457-617457100.17497.343.17100.9198.073.17
2577764-57776493.73594.46
3577859-57785993.75094.40
4600576-60057697.43698.16
5604319-60431998.04398.77
6622128-622128100.932101.71
60min1620057-620057100.59698.112.51101.5099.002.53
2589182-58918295.58796.47
3584504-58450494.82895.63
4605416-60541698.22199.10
5609038-60903898.80899.70
6620338-620338100.642101.59
极限1623478-623478101.151100.021.09102.22101.071.12
2618328-618328100.316101.35
3604993-60499398.15299.12
4612404-61240499.355100.40
5620312-620312100.637101.69
6619580-619580100.519101.63
恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DC033-12306002对照品来源分装对照品使用方法直接使用
对照品含量(%)98.99对照品水分(%)0对照品稀释倍数400
标示量(mg)25供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.285639315637625636575635545639025637610.03
210.215660705664725662710.06
单位质量响应值RSD%判断
54840.5655462.390.80数据可信
供试品溶液-2024052911批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1457999-45799973.98769.977.3273.9969.977.32
2444479-44447971.80371.80
3427441-42744169.05069.05
4423807-42380768.46368.46
5466789-46678975.40775.41
6378140-37814061.08661.09
10min1556192-55619289.84987.223.7589.9787.343.75
2542297-54229787.60587.72
3543159-54315987.74487.86
4546802-54680288.33388.45
5551082-55108289.02489.15
6500013-50001380.77480.88
15min1581326-58132693.91091.783.6194.1892.043.61
2561047-56104790.63490.90
3575710-57571093.00293.26
4575445-57544592.96093.22
5585331-58533194.55794.83
6529866-52986685.59785.83
20min1589665-58966595.25793.683.4295.6994.103.42
2571306-57130692.29192.71
3585555-58555594.59395.01
4589637-58963795.25295.67
5599266-59926696.80897.24
6544022-54402287.88388.26
30min1596700-59670096.39395.392.6296.9895.962.63
2581642-58164293.96194.53
3594737-59473796.07696.65
4599774-59977496.89097.46
5606362-60636297.95498.55
6563664-56366491.05691.58
45min1601058-60105897.09796.412.2097.8597.142.21
2586830-58683094.79995.53
3599676-59967696.87497.61
4608247-60824798.25999.00
5609290-60929098.42799.18
6575743-57574393.00893.69
60min1603106-60310697.42896.881.9198.3497.771.92
2589990-58999095.30996.19
3601480-60148097.16598.06
4609977-60997798.53899.44
5611374-61137498.76499.68
6582406-58240694.08494.92
极限1620028-620028100.16299.271.60101.23100.321.61
2606351-60635197.95299.00
3619467-619467100.071101.13
4620986-620986100.316101.38
5621865-621865100.458101.54
6598310-59831096.65397.64
恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DC033-12306002对照品来源分装对照品使用方法直接使用
对照品含量(%)98.99对照品水分(%)0对照品稀释倍数400
标示量(mg)25供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.285641715639755640185638115638945639740.03
210.215660465664155662300.05
单位质量响应值RSD%判断
54861.2855458.370.77数据可信
供试品溶液-2024053011批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1437827-43782770.71767.126.3170.7267.126.31
2446835-44683572.17272.17
3408882-40888266.04266.04
4426476-42647668.88468.88
5378652-37865261.15961.16
6394645-39464563.74363.74
10min1542226-54222687.58086.322.9387.7086.432.93
2549549-54954988.76388.88
3528522-52852285.36685.48
4546848-54684888.32688.44
5531923-53192385.91686.02
6507349-50734981.94782.05
15min1568751-56875191.86491.463.1892.1391.723.18
2580235-58023593.71993.99
3555069-55506989.65489.91
4577203-57720393.22993.49
5580885-58088593.82494.07
6535353-53535386.47086.71
20min1580206-58020693.71493.373.3694.1393.783.36
2590843-59084395.43295.86
3565988-56598891.41891.82
4589811-58981195.26695.68
5596579-59657996.35996.76
6545034-54503488.03388.42
30min1592248-59224895.65995.222.7096.2395.782.70
2594588-59458896.03796.62
3579411-57941193.58694.14
4602634-60263497.33797.91
5605364-60536497.77898.34
6562954-56295490.92891.46
45min1609530-60953098.45196.882.2799.1897.602.28
2600665-60066597.01997.76
3588504-58850495.05595.76
4613435-61343599.08199.82
5607918-60791898.19098.92
6578629-57862993.46094.14
60min1615674-61567499.44397.611.88100.3498.491.88
2603485-60348597.47498.38
3593420-59342095.84996.72
4615521-61552199.418100.32
5609072-60907298.37799.27
6588747-58874795.09495.93
极限1627033-627033101.27899.861.00102.34100.911.00
2609364-60936498.42499.49
3619036-61903699.986101.01
4620485-620485100.220101.29
5620216-620216100.177101.23
6613493-61349399.091100.09
点击查看处理图标(自动生成)
　
原始图谱下载图谱(姜进硙 于 2024-06-25 20:30:43 完成)
生成报告数据部分(等待生成报告)
Current page cost:44 ms