磷酸西格列汀片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101546-202101对照品来源中检院对照品使用方法直接使用
对照品含量(%)96.5对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.8061
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.171939361938621938191938261937341938350.04
213.241944641940741942690.15
单位质量响应值RSD%判断
14717.9214672.890.22数据可信
供试品溶液-2022030401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1200618-20061895.57695.630.7695.5895.630.76
2198998-19899894.80494.80
3199956-19995695.26095.26
4203533-20353396.96596.96
5200478-20047895.50995.51
6200859-20085995.69195.69
10min1204744-20474497.54297.690.7097.7097.850.71
2203326-20332696.86697.02
3204222-20422297.29397.45
4207479-20747998.84499.01
5204789-20478997.56397.72
6205768-20576898.02998.19
15min1205313-20531397.81398.040.7698.1398.360.76
2204295-20429597.32897.65
3204622-20462297.48397.80
4208508-20850899.33599.66
5205431-20543197.86998.19
6206625-20662598.43898.76
20min1205228-20522897.77298.050.7598.2698.540.75
2204707-20470797.52498.01
3204669-20466997.50697.99
4208625-20862599.39099.88
5205160-20516097.74098.22
6206502-20650298.37998.87
30min1204969-20496997.64997.980.7898.3098.630.78
2204500-20450097.42598.07
3204442-20444297.39898.04
4208650-20865099.402100.06
5205246-20524697.78198.43
6206152-20615298.21298.86
45min1204598-20459897.47297.830.8298.2898.640.82
2204031-20403197.20298.01
3204265-20426597.31398.12
4208401-20840199.284100.11
5204646-20464697.49598.31
6206146-20614698.20999.02
极限1205179-20517997.74997.800.7998.7298.770.79
2204523-20452397.43698.40
3203695-20369597.04298.01
4208191-20819199.184100.17
5204263-20426397.31298.29
6205822-20582298.05599.03
磷酸西格列汀片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101546-202101对照品来源中检院对照品使用方法直接使用
对照品含量(%)96.5对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.8061
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.171935031935461934291935491935471935150.03
213.241937741937481937610.01
单位质量响应值RSD%判断
14693.6214634.520.29数据可信
供试品溶液-2022030401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1202057-20205796.46795.151.1896.4795.141.18
2199835-19983595.40695.41
3200543-20054395.74495.74
4195219-19521993.20393.20
5198323-19832394.68594.68
6199758-19975895.37095.37
10min1206171-20617198.43197.191.1098.5997.351.10
2202083-20208396.48096.64
3205321-20532198.02698.19
4200346-20034695.65095.81
5202602-20260296.72796.89
6204862-20486297.80697.97
15min1206557-20655798.61697.611.3098.9497.931.30
2202390-20239096.62696.95
3207835-20783599.22699.55
4200796-20079695.86596.18
5203643-20364397.22497.54
6205460-20546098.09298.41
20min1206273-20627398.48097.521.1898.9798.011.18
2202547-20254796.70197.18
3205769-20576998.23998.73
4200701-20070195.82096.29
5203570-20357097.19097.67
6206760-20676098.71399.20
30min1206443-20644398.56197.381.0999.2198.021.08
2202589-20258996.72197.36
3205677-20567798.19698.85
4200435-20043595.69396.33
5203728-20372897.26597.91
6204878-20487897.81498.46
45min1206082-20608298.38997.271.0899.2198.081.08
2202009-20200996.44497.25
3205329-20532998.02998.85
4200374-20037495.66496.46
5203544-20354497.17797.98
6205069-20506997.90598.72
极限1207536-20753699.08397.301.30100.0698.271.30
2201994-20199496.43797.40
3205062-20506297.90298.88
4199944-19994495.45896.41
5203503-20350397.15898.12
6204772-20477297.76398.74
磷酸西格列汀片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101546-202101对照品来源中检院对照品使用方法直接使用
对照品含量(%)96.5对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.8061
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.171937321938161937781936511937501937450.04
213.241949741950481950110.03
单位质量响应值RSD%判断
14711.0914728.930.09数据可信
供试品溶液-2022030501批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1199898-19989895.07392.932.3695.0792.932.36
2195844-19584493.14593.15
3197176-19717693.77993.78
4187968-18796889.39989.40
5192118-19211891.37391.37
6199380-19938094.82794.83
10min1204881-20488197.44395.721.7397.6095.871.73
2200468-20046895.34595.50
3202428-20242896.27796.43
4196510-19651093.46293.61
5198242-19824294.28694.44
6204962-20496297.48297.64
15min1206109-20610998.02796.251.6498.3596.561.64
2201842-20184295.99896.31
3203310-20331096.69697.01
4197811-19781194.08194.39
5199497-19949794.88395.19
6205610-20561097.79098.11
20min1206778-20677898.34696.371.7098.8396.841.70
2201980-20198096.06496.54
3203449-20344996.76297.24
4198142-19814294.23894.70
5199485-19948594.87795.34
6205879-20587997.91898.40
30min1206547-20654798.23696.361.7098.8897.001.70
2202205-20220596.17196.80
3203552-20355296.81197.45
4197974-19797494.15894.78
5199434-19943494.85395.48
6205917-20591797.93698.58
45min1206631-20663198.27696.311.7799.0997.111.77
2202014-20201496.08096.87
3203247-20324796.66697.47
4197547-19754793.95594.73
5199542-19954294.90495.69
6206016-20601697.98398.79
极限1207526-20752698.70196.461.8899.6897.411.89
2202593-20259396.35597.31
3203335-20333596.70897.67
4197512-19751293.93994.87
5199621-19962194.94295.88
6206257-20625798.09899.07
磷酸西格列汀片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101546-202101对照品来源中检院对照品使用方法直接使用
对照品含量(%)96.5对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.8061
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.171947581946461947971946771949041947560.06
213.241951901951791951840.01
单位质量响应值RSD%判断
14787.8514741.990.22数据可信
供试品溶液-2022030501批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1201419-20141995.50696.601.2995.5196.601.29
2202448-20244895.99495.99
3207315-20731598.30198.30
4206801-20680198.05898.06
5201760-20176095.66795.67
6202675-20267596.10196.10
10min1206057-20605797.70598.931.2997.8699.091.29
2207286-20728698.28898.45
3212404-212404100.714100.88
4211624-211624100.344100.51
5207017-20701798.16098.32
6207399-20739998.34198.50
15min1206978-20697898.14299.231.2698.4699.551.26
2207760-20776098.51298.84
3212890-212890100.945101.28
4212331-212331100.680101.01
5207563-20756398.41998.74
6208091-20809198.66998.99
20min1206724-20672498.02199.211.2898.5199.701.28
2208035-20803598.64399.13
3212898-212898100.949101.45
4212323-212323100.676101.17
5207617-20761798.44598.93
6207770-20777098.51799.01
30min1206638-20663897.98099.181.2698.6399.841.26
2207883-20788398.57199.22
3212777-212777100.891101.56
4212206-212206100.620101.29
5207491-20749198.38599.04
6208042-20804298.64699.30
45min1206480-20648097.90599.011.2198.7299.831.21
2207621-20762198.44699.26
3212261-212261100.647101.48
4211762-211762100.410101.24
5207303-20730398.29699.11
6207404-20740498.34499.16
极限1207085-20708598.19299.021.0899.17100.001.08
2207784-20778498.52499.50
3211849-211849100.451101.46
4211580-211580100.324101.32
5207225-20722598.25999.24
6207446-20744698.36399.34
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2024-01-23 11:49:01 完成)
生成报告数据部分下载报告( 于 2026-01-02 02:02:41 完成)
Current page cost:71 ms