枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.412443442444202445142442742444192443940.04
217.42440622436082438350.14
单位质量响应值RSD%判断
14037.5614013.510.13数据可信
长期30℃12月-供试品溶液-EW4436批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1267860-26786096.70297.391.5896.7097.391.58
2275011-27501199.28499.28
3273884-27388498.87798.88
4263381-26338195.08595.09
5269925-26992597.44897.45
6268567-26856796.95796.96
10min1270122-27012297.51998.351.6297.6898.511.62
2277400-277400100.146100.31
3275991-27599199.63899.80
4265537-26553795.86496.02
5274479-27447999.09299.25
6270963-27096397.82297.98
15min1269727-26972797.37698.221.7797.7098.551.77
2277958-277958100.348100.68
3276481-27648199.814100.15
4265068-26506895.69496.01
5273373-27337398.69299.02
6269777-26977797.39497.72
20min1269813-26981397.40798.131.7897.8998.621.78
2277550-277550100.200100.70
3276427-27642799.795100.29
4264623-26462395.53496.01
5272935-27293598.53499.03
6269487-26948797.29097.78
30min1268766-26876697.02998.031.6997.6898.681.69
2276659-27665999.879100.55
3275992-27599299.638100.30
4265397-26539795.81396.45
5273675-27367598.80199.46
6268688-26868897.00197.65
45min1270670-27067097.71798.041.8798.5398.861.87
2278164-278164100.422101.26
3276369-27636999.774100.60
4264111-26411195.34996.15
5270814-27081497.76998.59
6269336-26933697.23598.05
极限1271511-27151198.02098.692.2898.9999.672.27
2282716-282716102.065103.07
3277824-277824100.299101.30
4265291-26529195.77596.73
5273576-27357698.76699.75
6269279-26927997.21498.19
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