叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.14 9907999013989079880998985989590.11
210.089920498924990640.20
单位质量响应值RSD%判断
9759.279827.780.50数据可信
供试品溶液-24061901批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min115239-1523925.54425.002.7825.5424.992.78
215189-1518925.46025.46
314959-1495925.07525.07
414825-1482524.85024.85
515129-1512925.36025.36
614128-1412823.68223.68
10min123641-2364139.62842.023.7639.9142.293.73
225314-2531442.43242.71
324768-2476841.51741.80
425578-2557842.87543.15
526418-2641844.28344.56
624677-2467741.36441.63
15min127063-2706345.36450.726.1246.0951.466.05
231266-3126652.40953.16
329761-2976149.88650.63
432609-3260954.66055.41
530605-3060551.30152.07
630244-3024450.69651.42
20min120706-2070634.70853.4917.9435.9454.8017.58
232206-3220653.98555.32
332794-3279454.97056.26
436722-3672261.55562.91
535040-3504058.73560.08
634014-3401457.01558.30
30min128250-2825047.35462.2812.4948.9764.1812.35
238998-3899865.37067.31
336440-3644061.08262.99
441311-4131169.24771.29
539518-3951866.24168.24
638397-3839764.36266.28
45min126614-2661444.61165.6316.9146.7568.2216.60
243253-4325372.50275.16
339065-3906565.48268.07
445524-4552476.30979.12
539186-3918665.68568.42
641275-4127569.18671.82
60min125682-2568243.04968.7319.2945.6872.0518.90
243712-4371273.27176.74
340410-4041067.73671.05
448088-4808880.60784.27
544863-4486375.20178.66
643262-4326272.51775.92
90min122270-2227037.33069.4723.5740.4473.5522.94
245251-4525175.85180.13
341035-4103568.78472.85
449288-4928882.61887.17
546325-4632577.65181.95
644482-4448274.56278.77
极限130657-3065751.38877.1816.7554.9282.0416.58
248515-4851581.32286.45
346632-4663278.16682.99
451592-5159286.48091.95
549633-4963383.19688.36
649243-4924382.54387.58
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.14 9912299406995159926199252993110.16
210.089872998719987240.01
单位质量响应值RSD%判断
9793.989794.050.01数据可信
供试品溶液-24061901批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122087-2208737.02136.781.6837.0236.781.68
222282-2228237.34737.35
322212-2221237.23037.23
421544-2154436.11036.11
522126-2212637.08637.09
621421-2142135.90435.90
10min134076-3407657.11649.9539.0457.5350.3638.72
235134-3513458.88959.30
36086-608610.20110.61
433721-3372156.52156.92
535226-3522659.04359.46
634573-3457357.94958.35
15min141258-4125869.15470.291.7770.2071.251.63
242714-4271471.59472.66
342708-4270871.58472.11
441014-4101468.74569.77
542286-4228670.87771.94
641620-4162069.76070.80
20min145307-4530775.94077.271.3377.7579.011.29
246434-4643477.82979.69
346434-4643477.82979.15
445396-4539676.08977.88
546804-4680478.44980.31
646222-4622277.47479.29
30min149901-4990183.64085.061.1686.3087.671.07
250633-5063384.86787.60
351293-5129385.97488.16
450439-5043984.54287.18
551516-5151686.34789.07
650720-5072085.01387.69
45min154785-5478591.82790.570.9195.4194.121.01
254098-5409890.67594.35
353524-5352489.71392.86
453527-5352789.71893.30
554366-5436691.12494.81
653923-5392390.38294.01
60min155598-5559893.18992.020.7597.8096.570.74
254687-5468791.66296.34
354901-5490192.02196.16
454446-5444691.25895.83
554669-5466991.63296.33
655084-5508492.32896.96
90min155700-5570093.36093.832.9299.0099.412.56
254631-5463191.56897.27
359172-5917299.180104.34
455185-5518592.49798.09
555183-5518392.49498.21
656019-5601993.89599.55
极限156181-5618194.16692.430.95100.8599.060.91
254711-5471191.70398.42
355110-5511092.37198.63
454926-5492692.06398.68
554984-5498492.16098.91
654971-5497192.13898.84
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