枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.184670484694544673444683074670094678320.23
217.064660514667724664120.11
单位质量响应值RSD%判断
27231.2027339.510.29数据可信
供试品溶液-2024051712批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1531666-53166698.66496.431.5198.6696.431.50
2525419-52541997.50597.50
3515079-51507995.58695.59
4518661-51866196.25196.25
5517251-51725195.98995.99
6509702-50970294.58894.59
10min1536321-53632199.52897.711.5699.6997.881.56
2536297-53629799.52399.69
3523835-52383597.21197.37
4522362-52236296.93797.10
5524622-52462297.35797.52
6515833-51583395.72695.88
15min1537042-53704299.66297.891.5099.9998.221.50
2535139-53513999.30899.64
3528141-52814198.01098.33
4522062-52206296.88297.20
5526496-52649697.70598.03
6516131-51613195.78196.10
20min1535968-53596899.46297.821.4799.9698.301.47
2535660-53566099.40599.90
3527602-52760297.91098.39
4521044-52104496.69397.18
5525605-52560597.53998.02
6516781-51678195.90296.38
30min1535594-53559499.39397.731.59100.0698.381.58
2536510-53651099.563100.22
3526612-52661297.72698.37
4521248-52124896.73197.38
5524920-52492097.41298.06
6514946-51494695.56196.20
45min1536834-53683499.62397.811.56100.4598.621.56
2535393-53539399.356100.18
3527522-52752297.89598.71
4521990-52199096.86897.67
5525479-52547997.51698.33
6515071-51507195.58496.38
极限1537036-53703699.66098.021.24100.6598.991.24
2535743-53574399.421100.41
3525968-52596897.60798.58
4522633-52263396.98897.95
5522515-52251596.96697.94
6525158-52515897.45698.41
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