枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.184645514646394647364645494657374648420.11
217.064666184678274672220.19
单位质量响应值RSD%判断
27057.1627386.990.86数据可信
供试品溶液-2024051712批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1511722-51172295.18794.277.4195.1994.277.41
2521805-52180597.06297.06
3521513-52151397.00897.01
4514244-51424495.65695.66
5432587-43258780.46780.47
6538740-538740100.212100.21
10min1518964-51896496.53496.585.9396.6996.735.94
2529792-52979298.54898.71
3530118-53011898.60998.77
4537927-537927100.061100.22
5458239-45823985.23885.37
6540157-540157100.476100.64
15min1520980-52098096.90996.985.0297.2397.305.03
2530687-53068798.71499.04
3530439-53043998.66898.99
4537736-537736100.026100.35
5469540-46954087.34087.62
6538710-538710100.207100.54
20min1520747-52074796.86597.264.3497.3597.744.35
2529880-52988098.56499.05
3531060-53106098.78499.27
4537785-537785100.035100.53
5478635-47863589.03289.45
6539182-539182100.295100.80
30min1521753-52175397.05397.493.5597.7098.143.56
2529984-52998498.58499.24
3527939-52793998.20398.86
4537763-537763100.031100.69
5488491-48849190.86591.44
6538838-538838100.231100.90
45min1523595-52359597.39598.202.9498.2099.002.96
2537175-53717599.921100.74
3528569-52856998.32099.14
4538342-538342100.138100.96
5499195-49919592.85793.58
6540709-540709100.579101.41
极限1520912-52091296.89699.101.6397.86100.071.60
2529156-52915698.43099.42
3526441-52644197.92598.91
4536307-53630799.760100.75
5540909-540909100.616101.49
6542866-542866100.980101.98
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