枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.184668774660024666474666054670774666420.09
217.064687204685484686340.03
单位质量响应值RSD%判断
27161.9327469.750.80数据可信
供试品溶液-2024051713批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1533307-53330798.86197.081.5898.8697.081.58
2521047-52104796.58896.59
3533701-53370198.93498.93
4522016-52201696.76896.77
5512886-51288695.07595.08
6519132-51913296.23396.23
10min1543233-543233100.701100.013.95100.87100.173.95
2525139-52513997.34797.51
3580490-580490107.607107.77
4529814-52981498.21398.37
5523732-52373297.08697.24
6534524-53452499.08699.25
15min1547835-547835101.55498.771.88101.8999.101.88
2522757-52275796.90597.23
3535811-53581199.32599.67
4531134-53113498.45898.78
5521290-52129096.63396.95
6537988-53798899.728100.05
20min1536845-53684599.51798.441.38100.0298.941.38
2522743-52274396.90297.39
3536085-53608599.37699.89
4531498-53149898.52599.01
5521362-52136296.64697.13
6537756-53775699.685100.18
30min1535999-53599999.36098.511.31100.0399.171.32
2523889-52388997.11597.76
3535308-53530899.23299.91
4533020-53302098.80899.46
5521679-52167996.70597.35
6538579-53857999.838100.50
45min1535164-53516499.20598.601.26100.0499.421.27
2527236-52723697.73598.54
3535524-53552499.272100.11
4530880-53088098.41199.23
5521866-52186696.74097.54
6540678-540678100.227101.05
极限1534976-53497699.17098.731.16100.1799.721.16
2535635-53563599.292100.26
3532334-53233498.68099.69
4532373-53237398.68899.67
5521193-52119396.61597.58
6539248-53924899.962100.95
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