枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.184667384665454668264679684669994670150.12
217.064661554662084661820.01
单位质量响应值RSD%判断
27183.6427326.030.37数据可信
供试品溶液-2024051713批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1531924-53192498.82398.160.9298.8298.160.92
2519868-51986896.58396.58
3532507-53250798.93198.93
4530108-53010898.48598.49
5530283-53028398.51898.52
6525377-52537797.60697.61
10min1531798-53179898.79999.000.3998.9699.160.39
2531088-53108898.66798.83
3530420-53042098.54398.71
4534963-53496399.38799.55
5533645-53364599.14299.31
6535215-53521599.43499.60
15min1532649-53264998.95799.130.2999.2999.450.29
2531869-53186998.81299.14
3532474-53247498.92599.25
4533634-53363499.14099.47
5534889-53488999.37399.70
6535811-53581199.54599.87
20min1533016-53301699.02698.950.4199.5299.440.41
2531584-53158498.75999.25
3531635-53163598.76999.26
4530900-53090098.63299.13
5531658-53165898.77399.27
6536735-53673599.716100.21
30min1534419-53441999.28699.000.3899.9599.660.38
2531233-53123398.69499.35
3531104-53110498.67099.33
4534133-53413399.23399.89
5531013-53101398.65399.31
6535411-53541199.470100.13
45min1536149-53614999.60899.561.35100.43100.381.34
2529522-52952298.37699.20
3533107-53310799.04299.87
4549726-549726102.130102.95
5531500-53150098.74499.57
6535369-53536999.463100.29
极限1536152-53615299.60899.260.99100.60100.250.98
2530357-53035798.53299.51
3532967-53296799.016100.00
4542421-542421100.773101.77
5527468-52746897.99598.98
6536371-53637199.649100.64
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