叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.241004681006351002711001851004371003990.18
210.279974399988998660.18
单位质量响应值RSD%判断
9804.599724.050.59数据可信
供试品溶液-24060304批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19660-966016.24114.288.1916.2414.288.17
29020-902015.16515.16
38173-817313.74113.74
48190-819013.76913.77
57902-790213.28513.29
68013-801313.47213.47
10min17545-754512.68512.363.3612.8712.523.37
27350-735012.35712.53
37600-760012.77812.93
47332-733212.32712.48
56901-690111.60211.75
67397-739712.43612.59
15min17140-714012.00411.813.1612.3312.113.19
27246-724612.18212.49
37228-722812.15212.45
47017-701711.79712.09
56787-678711.41111.69
66731-673111.31711.60
20min16757-675711.36011.082.3011.8111.512.30
26618-661811.12711.57
36560-656011.02911.46
46390-639010.74311.16
56467-646710.87311.28
66764-676411.37211.79
30min16517-651710.95710.544.3311.5411.094.27
26696-669611.25811.82
36166-616610.36710.92
46106-610610.26610.81
56066-606610.19810.72
66056-605610.18210.72
45min16328-632810.63910.302.5611.3410.972.57
26116-611610.28310.97
36171-617110.37511.04
46172-617210.37711.03
55848-58489.83210.47
66126-612610.29910.95
60min16056-605610.1829.843.0111.0010.623.02
26005-600510.09610.90
35966-596610.03010.81
45695-56959.57510.34
55651-56519.50110.25
65742-57429.65410.42
90min15869-58699.8679.354.2710.8010.244.17
25727-57279.62910.54
35602-56029.41810.31
45549-55499.32910.21
55189-51898.7249.58
65423-54239.1179.99
极限15219-52198.77421.32145.749.8222.32139.13
25045-50458.4829.51
35199-51998.7419.74
45114-51148.5989.58
550415-5041584.76085.71
65110-51108.5919.57
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