叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.241004681006351002711001851004371003990.18
210.279974399988998660.18
单位质量响应值RSD%判断
9804.599724.050.59数据可信
供试品溶液-24060304批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124008-2400840.36338.034.3840.3638.034.38
222997-2299738.66438.66
322930-2293038.55138.55
421049-2104935.38935.39
522098-2209837.15237.15
622650-2265038.08038.08
10min136306-3630661.04058.283.4461.4958.703.44
233988-3398857.14257.57
335196-3519659.17359.60
432858-3285855.24355.64
534390-3439057.81858.23
635232-3523259.23459.66
15min142420-4242071.31969.362.0472.4570.432.05
240395-4039567.91468.98
340906-4090668.77369.86
440327-4032767.80068.81
541757-4175770.20471.26
641707-4170770.12071.20
20min145414-4541476.35274.562.5978.2776.402.59
243678-4367873.43475.25
344727-4472775.19777.05
442332-4233271.17172.93
545008-4500875.67077.51
644914-4491475.51277.37
30min148704-4870481.88479.662.0384.6582.332.04
246542-4654278.24980.88
346985-4698578.99481.68
446278-4627877.80580.36
548257-4825781.13283.81
647525-4752579.90182.60
45min152238-5223887.82584.212.4491.5087.762.42
248563-4856381.64785.15
349590-4959083.37386.94
449651-4965183.47686.89
550105-5010584.23987.82
650365-5036584.67688.26
60min152358-5235888.02785.022.1892.6889.512.16
249049-4904982.46486.88
349974-4997484.01988.51
450617-5061785.10089.44
550996-5099685.73790.25
650415-5041584.76089.29
90min152006-5200687.43585.111.6593.0790.541.66
249795-4979583.71889.05
349888-4988883.87489.30
450555-5055584.99690.28
551132-5113285.96691.43
650354-5035484.65890.13
极限151135-5113585.97184.321.1792.5790.701.21
249461-4946183.15689.41
350071-5007184.18290.54
450122-5012284.26890.50
550415-5041584.76091.18
649706-4970683.56889.98
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