塞来昔布胶囊项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号510141-202102对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152979769298491729784522979672297967829804980.09
210.193001476299527329983740.15
单位质量响应值RSD%判断
293645.12294246.710.15数据可信
供试品溶液-20211227批-pH12.0(内含1.0%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1943551-94355131.97138.7822.3931.9738.7822.38
21411997-141199747.84447.84
31392495-139249547.18347.18
41059629-105962935.90435.90
51275941-127594143.23443.23
6783741-78374126.55626.56
10min11845005-184500562.51666.7118.7062.5666.7718.70
22212484-221248474.96775.04
32585517-258551787.60787.68
41602332-160233254.29354.35
51882551-188255163.78863.85
61684962-168496257.09357.13
15min12143345-214334572.62581.7815.3972.7781.9415.40
22748651-274865193.13593.32
32886465-288646597.80498.01
41885036-188503663.87264.01
52436622-243662282.56282.72
62381210-238121080.68480.81
20min12703310-270331091.59892.568.2491.8592.848.26
22904540-290454098.41798.74
32927414-292741499.19299.54
42306767-230676778.16278.39
52771765-277176593.91894.20
62776380-277638094.07494.32
30min13133611-3133611106.179100.083.02106.57100.503.00
22913364-291336498.71699.19
32924460-292446099.09299.59
42894954-289495498.09298.44
52926553-292655399.16399.59
62928628-292862899.23399.62
45min13149381-3149381106.713100.383.11107.26100.953.09
22917172-291717298.84599.46
32925519-292551999.12899.77
42910344-291034498.61499.11
52934542-293454299.433100.01
62938633-293863399.572100.11
60min13148536-3148536106.684100.383.13107.39101.103.10
22909479-290947998.58499.35
32926432-292643299.15999.95
42904671-290467198.42199.06
52945482-294548299.804100.53
62940780-294078099.645100.33
极限13152710-3152710106.826100.653.04107.69101.523.02
22926951-292695199.176100.09
32943688-294368899.743100.69
42912556-291255698.68999.48
52942805-294280599.713100.59
62943142-294314299.725100.56
塞来昔布胶囊项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号510141-202102对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152997165299497929959992996418297207529913270.37
210.192972734297064829716910.05
单位质量响应值RSD%判断
294712.02291628.160.75数据可信
供试品溶液-20211227批-pH12.0(内含1.0%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1974788-97478833.11837.3925.0933.1237.3825.09
21221268-122126841.49241.49
31323169-132316944.95444.95
41184541-118454140.24440.24
51301872-130187244.23044.23
6596947-59694720.28120.28
10min11926499-192649965.45269.529.7365.5069.589.73
21916888-191688865.12565.19
32214800-221480075.24675.31
41960615-196061566.61166.67
52371686-237168680.57780.64
61887739-188773964.13564.17
15min12653832-265383290.16290.394.4390.3190.554.44
22763796-276379693.89894.06
32703037-270303791.83492.01
42522528-252252885.70185.86
52797861-279786195.05695.24
62522789-252278985.71085.84
20min12839900-283990096.484100.424.7496.77100.724.72
23217521-3217521109.313109.61
32898330-289833098.46998.79
42869965-286996597.50597.79
52902396-290239698.60798.94
63006597-3006597102.147102.40
30min12992412-2992412101.665103.104.57102.09103.544.54
23257570-3257570110.674111.14
32917693-291769399.12799.59
42960105-2960105100.568101.00
52927488-292748899.46099.94
63151709-3151709107.077107.49
45min13082805-3082805104.736103.434.83105.32104.044.80
23250920-3250920110.448111.08
32907066-290706698.76699.38
42931686-293168699.602100.19
52920615-292061599.22699.85
63173727-3173727107.825108.39
60min12985426-2985426101.428102.574.74102.17103.334.72
23248076-3248076110.351111.15
32899823-289982398.52099.28
42925746-292574699.400100.14
52914290-291429099.01199.79
63140963-3140963106.712107.44
极限12981821-2981821101.306102.494.74102.20103.404.72
23244691-3244691110.236111.20
32898086-289808698.46199.37
42925798-292579899.402100.29
52910141-291014198.87099.79
63140155-3140155106.685107.58
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢鑫慧 于 2024-07-02 17:00:56 完成)
生成报告数据部分(等待生成报告)
Current page cost:46 ms