阿齐沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数3125
标示量(mg)5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.328788487888879158776587840878580.07
211.398902689013890200.02
单位质量响应值RSD%判断
7761.317815.630.50数据可信
供试品溶液-8145761批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min160710-6071062.99662.273.0763.0062.273.07
261085-6108563.38563.39
359129-5912961.35661.36
462767-6276765.13165.13
558514-5851460.71760.72
657855-5785560.03460.03
10min173806-7380676.58578.701.7976.9479.051.79
275763-7576378.61678.97
376093-7609378.95879.30
477881-7788180.81481.18
575127-7512777.95678.29
676393-7639379.27079.60
15min181861-8186184.94484.132.5885.7284.922.57
282617-8261785.72886.52
382180-8218085.27586.05
482701-8270185.81586.63
577477-7747780.39581.16
679644-7964482.64383.42
20min184516-8451687.69987.621.8688.9588.871.85
286636-8663689.89891.16
384200-8420087.37188.62
485696-8569688.92390.21
582366-8236685.46886.68
683239-8323986.37487.61
30min189191-8919192.55092.051.7394.2893.791.73
291148-9114894.58096.34
388319-8831991.64593.38
489369-8936992.73494.52
587159-8715990.44192.13
687095-8709590.37592.09
45min192927-9292796.42695.511.1098.6897.751.10
292834-9283496.33098.62
392268-9226895.74397.99
492167-9216795.63897.93
591876-9187695.33697.53
690164-9016493.55995.77
60min194570-9457098.13197.310.92100.92100.090.91
293411-9341196.92999.75
393561-9356197.08499.86
494367-9436797.921100.75
594428-9442897.984100.71
692324-9232495.80198.54
极限191952-9195295.41598.141.8598.74101.461.79
293091-9309196.59799.96
394845-9484598.417101.74
496503-96503100.137103.51
596082-9608299.700102.97
694971-9497198.547101.81
阿齐沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数3125
标示量(mg)5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.328780287799877938776787768877860.02
211.398841188489884500.07
单位质量响应值RSD%判断
7754.957765.580.10数据可信
供试品溶液-8145761批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min159140-5914061.58961.732.3861.5961.732.38
258381-5838160.79960.80
359288-5928861.74361.74
461031-6103163.55963.56
557223-5722359.59359.59
660613-6061363.12363.12
10min174107-7410777.17678.221.8877.5278.561.87
274385-7438577.46677.80
375242-7524278.35878.70
477768-7776880.98981.34
573990-7399077.05477.39
675142-7514278.25478.60
15min180412-8041283.74283.721.2984.5184.501.29
280036-8003683.35184.12
379993-7999383.30684.08
482420-8242085.83486.64
579567-7956782.86283.62
679923-7992383.23384.02
20min183907-8390787.38286.620.8488.6287.860.84
282031-8203185.42886.66
382847-8284786.27887.52
483704-8370487.17188.45
583005-8300586.44387.66
683555-8355587.01688.26
30min188338-8833891.99790.401.4593.7292.131.42
285087-8508788.61190.32
386712-8671290.30392.02
486363-8636389.94091.70
588196-8819691.84993.55
686158-8615889.72691.46
45min193055-9305596.90994.211.9099.1496.441.85
288975-8897592.66094.86
390108-9010893.84096.06
488890-8889092.57194.84
592057-9205795.87098.08
689722-8972293.43895.67
60min193726-9372697.60896.272.63100.3899.022.56
293038-9303896.89199.60
391259-9125995.03997.78
489814-8981493.53496.31
596345-96345100.335103.08
690448-9044894.19496.94
极限197435-97435101.470100.291.57104.78103.571.54
294491-9449198.404101.66
394826-9482698.753102.02
496926-96926100.940104.24
598294-98294102.365105.66
695816-9581699.784103.06
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