枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.272408672408682419942414832415992413620.21
217.232407792420282414040.37
单位质量响应值RSD%判断
13975.8014010.680.18数据可信
供试品溶液-2024051613批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1273851-27385199.09398.431.5399.0998.431.53
2272006-27200698.42698.43
3272139-27213998.47498.47
4266963-26696396.60196.60
5268482-26848297.15197.15
6278716-278716100.854100.85
10min1276961-276961100.21999.771.39100.3899.941.39
2274769-27476999.42599.59
3274724-27472499.40999.57
4271457-27145798.22798.39
5273824-27382499.08499.25
6282616-282616102.265102.43
15min1276940-276940100.211100.071.13100.54100.401.13
2274259-27425999.24199.57
3275390-27539099.65099.98
4277346-277346100.358100.68
5273254-27325498.87799.20
6282055-282055102.062102.40
20min1276285-27628599.974100.331.69100.47100.831.68
2273819-27381999.08299.58
3274574-27457499.35599.85
4284250-284250102.856103.35
5272877-27287798.74199.23
6281798-281798101.969102.48
30min1275807-27580799.80199.411.33100.47100.081.33
2273297-27329798.89399.55
3274123-27412399.19299.85
4271173-27117398.12498.79
5272509-27250998.60899.26
6281475-281475101.852102.53
45min1275793-27579399.79699.111.27100.6399.941.26
2272532-27253298.61699.44
3273386-27338698.92599.75
4270179-27017997.76598.59
5271648-27164898.29699.12
6279820-279820101.253102.10
极限1275370-27537099.64399.001.37100.6499.991.37
2272462-27246298.59199.58
3272932-27293298.76199.75
4269371-26937197.47298.46
5271296-27129698.16999.15
6280082-280082101.348102.37
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