塞来昔布胶囊项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号510141-202102对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.89 2980031298256429806782980907297518329798730.10
29.942974678297460929746440.01
单位质量响应值RSD%判断
301301.62299259.960.49数据可信
供试品溶液-8145830批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min120568-205680.6820.7518.320.680.7518.63
226752-267520.8870.89
321109-211090.7000.70
419093-190930.6330.63
528861-288610.9570.96
619320-193200.6410.64
10min138834-388341.2881.296.191.291.296.28
240491-404911.3431.34
339614-396141.3141.32
435316-353161.1711.17
541721-417211.3841.39
636696-366961.2171.22
15min141597-415971.3801.391.511.381.391.54
242417-424171.4071.41
341901-419011.3901.39
440892-408921.3561.36
542645-426451.4151.42
641715-417151.3841.39
20min142102-421021.3961.390.891.401.390.85
242342-423421.4041.41
341669-416691.3821.39
441562-415621.3791.38
541604-416041.3801.39
641319-413191.3711.38
30min140703-407031.3501.361.291.361.361.38
240962-409621.3591.37
340943-409431.3581.37
441537-415371.3781.38
541250-412501.3681.38
640002-400021.3271.33
45min139284-392841.3031.322.011.311.331.93
240417-404171.3411.35
340414-404141.3411.35
440264-402641.3361.34
540386-403861.3401.35
638526-385261.2781.29
60min138592-385921.2801.292.561.291.302.55
239435-394351.3081.32
340412-404121.3401.35
438838-388381.2881.30
538805-388051.2871.30
637376-373761.2401.25
极限138783-387831.2861.272.861.301.292.73
238889-388891.2901.30
340068-400681.3291.34
437523-375231.2451.26
538047-380471.2621.28
636992-369921.2271.24
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