氯沙坦钾苯磺酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号LQSA-4-06220206对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.778199688206608206118202738205568204140.04
29.828247368249798248580.03
单位质量响应值RSD%判断
83972.7783997.760.03数据可信
供试品溶液-1批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min116636-166361.7791.805.531.781.805.43
215290-152901.6351.64
317587-175871.8811.88
417861-178611.9101.91
516439-164391.7581.76
617178-171781.8371.84
10min133171-331713.5483.595.063.553.595.06
231076-310763.3233.33
334698-346983.7113.71
435925-359253.8423.85
532544-325443.4803.48
633925-339253.6283.63
15min147836-478365.1165.155.745.125.165.79
244661-446614.7764.78
350851-508515.4385.45
451962-519625.5575.57
546205-462054.9424.95
647619-476195.0935.10
20min161164-611646.5416.476.416.566.496.41
255732-557325.9605.98
364529-645296.9016.92
465043-650436.9566.98
556672-566726.0616.08
659892-598926.4056.42
30min192165-921659.8579.348.889.899.378.86
278169-781698.3608.39
397343-9734310.41110.44
492159-921599.8569.89
579508-795088.5038.53
684516-845169.0399.07
45min1148677-14867715.90115.586.0915.9515.626.09
2134827-13482714.41914.46
3158956-15895617.00017.05
4150673-15067316.11416.16
5138253-13825314.78614.83
6142645-14264515.25615.30
60min1194740-19474020.82720.983.1320.9021.053.15
2187101-18710120.01020.07
3195689-19568920.92821.00
4205545-20554521.98222.06
5194409-19440920.79220.86
6199732-19973221.36121.43
120min1318769-31876934.09136.469.1834.2036.569.15
2322031-32203134.44034.54
3338095-33809536.15836.27
4402572-40257243.05443.16
5337823-33782336.12936.23
6326004-32600434.86534.97
极限1691778-69177873.98476.294.1074.1576.454.09
2743038-74303879.46679.62
3666379-66637971.26771.44
4737260-73726078.84879.03
5725129-72512977.55177.71
6716305-71630576.60776.77
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