左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.741822561820371823441825841818221822090.17
217.071879341881181880260.07
单位质量响应值RSD%判断
10884.6511015.000.85数据可信
供试品溶液-8153342批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1225594-225594104.068103.812.50104.07103.812.50
2227255-227255104.834104.83
3220582-220582101.756101.76
4226422-226422104.450104.45
5233272-233272107.610107.61
6217122-217122100.160100.16
10min1224310-224310103.476103.952.89104.63105.102.89
2228854-228854105.572106.74
3220951-220951101.926103.06
4225615-225615104.078105.24
5235555-235555108.663109.86
6216699-21669999.965101.08
15min1223317-223317103.017102.792.61105.32105.102.61
2226104-226104104.303106.64
3219377-219377101.200103.46
4220958-220958101.929104.25
5231998-231998107.022109.43
6215226-21522699.285101.51
20min1221306-221306102.090101.992.71105.54105.442.71
2224767-224767103.686107.18
3217669-217669100.412103.80
4220718-220718101.818105.27
5229787-229787106.002109.59
6212271-21227197.922101.25
30min1220602-220602101.765101.222.58106.35105.812.58
2222128-222128102.469107.12
3214542-21454298.969103.47
4220791-220791101.852106.43
5227151-227151104.786109.56
6211338-21133897.491101.91
45min1218041-218041100.58499.962.34106.30105.672.35
2219031-219031101.040106.83
3212664-21266498.103103.71
4214955-21495599.160104.87
5224747-224747103.677109.61
6210665-21066597.181102.68
极限1214150-21415098.78999.082.09105.62105.902.11
2217574-217574100.368107.28
3213501-21350198.489105.18
4213532-21353298.504105.32
5221633-221633102.241109.33
6208342-20834296.109102.69
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