左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.29 1986521982981995001982021986711986650.26
216.301983271982281982780.04
单位质量响应值RSD%判断
12195.5212164.290.19数据可信
供试品溶液-24062101批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
15min161104-6110451.47263.1020.3851.4763.1020.38
261054-6105451.43051.43
358698-5869849.44649.45
461910-6191052.15152.15
559864-5986450.42850.43
659472-5947250.09850.10
789320-8932075.24175.24
890563-9056376.28876.29
987167-8716773.42773.43
1089661-8966175.52875.53
1188615-8861574.64774.65
1291511-9151177.08677.09
30min1100350-10035084.53242.82104.4885.1043.52102.47
2103556-10355687.23387.80
399087-9908783.46884.02
4101213-10121385.25985.84
5101730-10173085.69586.25
6104088-10408887.68188.24
7-0.0000.84
8-0.0000.85
9-0.0000.82
10-0.0000.84
11-0.0000.83
12-0.0000.86
45min1-0.0000.00-1.511.1830.03
2-0.0001.54
3-0.0001.48
4-0.0001.53
5-0.0001.51
6-0.0001.53
7-0.0000.84
8-0.0000.85
9-0.0000.82
10-0.0000.84
11-0.0000.83
12-0.0000.86
左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.29 1968561971161968241970031970711969740.07
216.301961481956691959080.18
单位质量响应值RSD%判断
12091.7112018.900.43数据可信
供试品溶液-24062101批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
15min148204-4820441.02642.6111.8741.0342.6111.87
246725-4672539.76739.77
347428-4742840.36540.37
446076-4607639.21539.21
560111-6011151.16051.16
657445-5744548.89148.89
756686-5668648.24548.24
856710-5671048.26548.27
942751-4275136.38536.38
1044305-4430537.70737.71
1145849-4584939.02139.02
1248434-4843441.22141.22
30min157085-5708548.58456.6524.7349.0457.1224.62
255850-5585047.53347.97
356401-5640148.00248.45
455232-5523247.00747.44
590489-9048977.01477.58
686363-8636373.50274.05
785538-8553872.80073.34
891818-9181878.14578.68
956486-5648648.07448.48
1049448-4944842.08442.50
1155832-5583247.51847.95
1258161-5816149.50049.96
45min160802-6080251.74861.6627.8752.7462.7627.71
258658-5865849.92350.89
359123-5912350.31951.30
456917-5691748.44149.40
5101629-10162986.49587.92
697225-9722582.74784.11
796322-9632281.97883.32
8102721-10272187.42488.83
961839-6183952.63053.57
1060701-6070151.66252.55
1161373-6137352.23453.20
1252090-5209044.33345.34
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