叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.141004941005191005891003211002071004260.16
210.089941499483994480.05
单位质量响应值RSD%判断
9903.949865.870.28数据可信
供试品溶液-24061901批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1114589-11458995.15097.381.6295.1597.381.62
2117066-11706697.20797.21
3120395-12039599.97199.97
4116787-11678796.97596.98
5117979-11797997.96597.97
6116801-11680196.98796.99
10min1116146-11614696.44397.641.0696.6097.801.06
2117054-11705497.19797.36
3119528-11952899.25199.42
4117400-11740097.48497.65
5118571-11857198.45798.62
6116814-11681496.99897.16
15min1115787-11578796.14597.581.2496.4697.901.24
2117084-11708497.22297.55
3119826-11982699.49999.83
4116857-11685797.03397.36
5118616-11861698.49498.82
6116885-11688597.05797.38
20min1115412-11541295.83397.141.2596.3197.631.26
2116552-11655296.78097.27
3119463-11946399.19799.70
4116770-11677096.96197.45
5117810-11781097.82598.32
6115925-11592596.25996.74
30min1115095-11509595.57097.121.4196.2197.771.40
2116393-11639396.64897.30
3118905-11890598.73499.40
4115974-11597496.30096.95
5119079-11907998.87899.53
6116324-11632496.59197.24
45min1114688-11468895.23296.661.3296.0397.461.32
2115885-11588596.22697.03
3118868-11886898.70399.53
4115668-11566896.04696.85
5117592-11759297.64498.46
6115712-11571296.08396.89
极限1114189-11418994.81896.271.3995.7897.241.38
2115516-11551695.92096.89
3118510-11851098.40699.40
4114851-11485195.36896.34
5117164-11716497.28898.27
6115393-11539395.81896.78
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