叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.141255661125556812557351255234125533612555070.02
210.081253014125226312526380.05
单位质量响应值RSD%判断
123817.26124269.640.26数据可信
供试品溶液-23FA408批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min157848-578487.6568.787.277.668.787.27
272147-721479.5489.55
368614-686149.0809.08
466437-664378.7928.79
568021-680219.0029.00
664787-647878.5748.57
10min1119506-11950615.81617.445.3215.9017.535.33
2140264-14026418.56318.67
3135811-13581117.97318.07
4130300-13030017.24417.34
5133680-13368017.69117.79
6130932-13093217.32817.42
15min1165270-16527021.87224.125.0222.1324.415.03
2192373-19237325.45925.77
3186975-18697524.74425.05
4181891-18189124.07224.36
5182705-18270524.17924.48
6184326-18432624.39424.68
20min1204479-20447927.06129.254.3327.5629.814.35
2233901-23390130.95531.55
3224963-22496329.77230.35
4221537-22153729.31829.88
5220895-22089529.23429.80
6220255-22025529.14929.71
30min1264351-26435134.98537.474.1835.7938.354.19
2297767-29776739.40740.35
3290350-29035038.42539.33
4285833-28583337.82738.71
5274940-27494036.38637.28
6285480-28548037.78138.66
45min1332616-33261644.01946.493.7345.2147.793.74
2368046-36804648.70850.08
3360091-36009147.65548.99
4354285-35428546.88648.19
5339588-33958844.94146.24
6352911-35291146.70548.01
60min1387237-38723751.24753.333.7652.9355.153.75
2423126-42312655.99757.92
3410345-41034554.30656.17
4407915-40791553.98455.81
5382964-38296450.68252.48
6406136-40613653.74955.57
90min1464185-46418561.43163.133.2963.6865.543.29
2496355-49635565.68868.23
3488846-48884664.69467.16
4475653-47565362.94865.37
5454357-45435760.13062.49
6482591-48259163.86766.29
极限1496020-49602065.64467.332.7268.5870.442.75
2525636-52563669.56372.83
3517294-51729468.45971.64
4516583-51658368.36571.49
5489417-48941764.77067.79
6507490-50749067.16270.29
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.141255376125606512556801255227125454212553780.05
210.081244876124734612461110.15
单位质量响应值RSD%判断
123804.54123622.120.11数据可信
供试品溶液-23FA408批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min173713-737139.78110.378.829.7810.378.83
283432-8343211.07111.07
389718-8971811.90511.91
472330-723309.5989.60
575413-7541310.00710.01
674320-743209.8629.86
10min1134102-13410217.79518.587.7717.9018.707.77
2146471-14647119.43619.56
3158942-15894221.09121.22
4129017-12901717.12017.23
5136859-13685918.16018.27
6134936-13493617.90518.01
15min1183744-18374424.38224.967.9024.6925.287.89
2202296-20229626.84327.18
3209919-20991927.85528.22
4174600-17460023.16823.47
5184227-18422724.44624.76
6173677-17367723.04623.35
20min1227402-22740230.17530.557.6830.7531.157.67
2245115-24511532.52533.16
3255144-25514433.85634.53
4218601-21860129.00729.56
5228765-22876530.35630.94
6206297-20629727.37427.94
30min1289732-28973238.44638.497.4439.3639.437.43
2311901-31190141.38742.39
3312914-31291441.52242.57
4282198-28219837.44638.32
5289291-28929138.38739.31
6254494-25449433.77034.64
45min1367351-36735148.74547.248.0850.0948.617.99
2384181-38418150.97852.44
3362036-36203648.04049.55
4356208-35620847.26748.56
5365835-36583548.54449.89
6300565-30056539.88341.13
60min1419552-41955255.67253.918.4957.5555.808.40
2442368-44236858.70060.72
3415182-41518255.09257.14
4408123-40812354.15555.97
5412070-41207054.67956.57
6340323-34032345.15946.85
90min1493820-49382065.52764.119.1668.0366.609.06
2528126-52812670.07972.76
3490573-49057365.09667.76
4486211-48621164.51766.94
5501935-50193566.60469.10
6398168-39816852.83455.02
极限1535392-53539271.04369.546.5674.2772.746.58
2566549-56654975.17878.63
3533644-53364470.81174.19
4524072-52407269.54172.68
5523075-52307569.40972.64
6461833-46183361.28264.06
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