依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DSMF-387-240606对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.051742711745991748351748951748681746940.16
210.091753791756771755280.13
单位质量响应值RSD%判断
17382.4917396.230.06数据可信
供试品溶液-X027068批-依折麦布-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19764-97645.0415.4314.745.045.4314.70
211302-113025.8355.83
311631-116316.0056.00
412610-126106.5106.51
58965-89654.6284.63
68843-88434.5654.57
10min117263-172638.9128.672.238.948.702.22
217128-171288.8438.87
316740-167408.6428.68
416835-168358.6918.73
516561-165618.5508.58
616242-162428.3858.41
15min117836-178369.2089.091.479.299.171.45
217814-178149.1979.28
317532-175329.0519.13
417152-171528.8558.94
517751-177519.1649.24
617540-175409.0559.13
20min117831-178319.2069.061.749.339.181.67
217752-177529.1659.30
317260-172608.9119.04
417070-170708.8138.95
517703-177039.1399.26
617619-176199.0969.22
30min117268-172688.9158.871.289.099.041.21
216997-169978.7758.96
317112-171128.8349.02
416873-168738.7118.89
517466-174669.0179.19
617316-173168.9409.11
45min117837-178379.2098.882.769.449.112.67
217090-170908.8239.06
316729-167298.6378.87
416713-167138.6288.86
517172-171728.8659.09
617695-176959.1359.36
60min116922-169228.7368.822.609.029.102.48
216735-167358.6408.92
316833-168338.6908.97
416744-167448.6448.92
517426-174268.9969.27
617818-178189.1999.47
极限117319-173198.9419.024.789.279.344.61
217656-176569.1159.44
316655-166558.5988.92
416479-164798.5088.83
518091-180919.3409.66
618650-186509.6289.95
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100590-202005对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.041477231483661486021485511482291482940.24
211.071488791491251490020.12
单位质量响应值RSD%判断
13432.4313459.980.15数据可信
供试品溶液-X027068批-阿托伐他汀钙-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min142917-4291726.36433.3433.9526.3633.3433.95
270804-7080443.49543.49
364628-6462839.70139.70
476223-7622346.82446.82
536848-3684822.63622.64
634217-3421721.02021.02
10min1125260-12526076.94779.957.6077.0980.147.65
2139169-13916985.49285.73
3139312-13931285.57985.80
4138284-13828484.94885.21
5120658-12065874.12074.25
6118197-11819772.60872.73
15min1154245-15424594.75395.371.8895.3396.001.92
2154375-15437594.83395.55
3161080-16108098.95299.65
4154824-15482495.10895.84
5153967-15396794.58295.12
6153053-15305394.02194.54
20min1161097-16109798.96299.771.43100.06100.921.40
2160213-16021398.41999.66
3165871-165871101.895103.14
4160443-16044398.56099.82
5164466-164466101.032102.09
6162340-16234099.726100.77
30min1159845-15984598.19399.892.2099.84101.602.15
2159665-15966598.08299.87
3167450-167450102.865104.68
4159906-15990698.230100.04
5166624-166624102.357103.98
6162116-16211699.588101.18
45min1165360-165360101.581100.921.29103.78103.181.22
2161939-16193999.479101.81
3165806-165806101.855104.24
4161452-16145299.180101.53
5166584-166584102.333104.53
6164519-164519101.064103.21
60min1161896-16189699.453100.632.73102.21103.462.65
2157600-15760096.81499.70
3168878-168878103.742106.69
4162182-16218299.628102.53
5169146-169146103.906106.67
6163201-163201100.254102.97
极限1162172-16217299.622100.941.60102.93104.321.56
2161890-16189099.449102.87
3167253-167253102.744106.27
4162106-16210699.582103.04
5167436-167436102.856106.19
6165022-165022101.373104.64
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DSMF-387-240606对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.051764351765371765651763801763921764620.05
210.091780761775441778100.22
单位质量响应值RSD%判断
17558.4117622.400.26数据可信
供试品溶液-X027068批-依折麦布-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min110259-102595.2365.9739.455.245.9739.44
220964-2096410.69910.70
310057-100575.1335.13
411021-110215.6255.62
59202-92024.6964.70
68679-86794.4294.43
10min116855-168558.60212.2774.848.6312.3074.74
260758-6075831.00931.07
317115-171158.7358.76
416917-169178.6348.67
516250-162508.2938.32
616345-163458.3428.37
15min117677-176779.02213.7684.829.1013.8684.66
273613-7361337.57037.80
317806-178069.0889.16
418332-183329.3569.44
517174-171748.7658.84
617128-171288.7428.81
20min117564-175648.96413.8183.229.0913.9883.09
272988-7298837.25137.69
318310-183109.3459.47
418766-187669.5789.71
517244-172448.8018.92
617443-174438.9029.02
30min116879-168798.61414.4593.728.7914.7093.42
282455-8245542.08242.73
317574-175748.9699.15
418433-184339.4089.59
517487-174878.9259.09
617030-170308.6928.86
45min117200-172008.77815.3599.799.0015.6999.37
291326-9132646.61047.49
319131-191319.7649.99
418461-184619.4229.66
517770-177709.0699.29
616602-166028.4738.69
60min117102-171028.72813.9389.099.0014.3588.95
276911-7691139.25340.39
317064-170648.7098.99
418173-181739.2759.56
517677-176779.0229.29
616824-168248.5868.85
极限116569-165698.45614.2792.368.7814.7692.10
280634-8063441.15342.51
317286-172868.8229.15
418625-186259.5069.85
517800-178009.0859.40
616820-168208.5848.90
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100590-202005对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.041497631497981496841496001496031496900.07
211.071512871506731509800.29
单位质量响应值RSD%判断
13558.8813638.660.42数据可信
供试品溶液-X027068批-阿托伐他汀钙-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144475-4447527.01526.5925.1227.0126.5925.12
236669-3666922.27322.27
339392-3939223.92723.93
465026-6502639.49839.50
542334-4233425.71425.71
634799-3479921.13721.14
10min1126985-12698577.13274.846.3777.2874.996.41
2112149-11214968.12168.24
3120158-12015872.98673.12
4134811-13481181.88682.11
5126216-12621676.66576.81
6118939-11893972.24572.36
15min1153658-15365893.33492.082.8193.9192.642.85
2148524-14852490.21590.72
3148862-14886290.42190.96
4158962-15896296.55697.23
5151772-15177292.18892.76
6147758-14775889.75090.27
20min1160166-16016697.28797.911.6798.3898.991.72
2159079-15907996.62797.63
3159570-15957096.92597.97
4166129-166129100.909102.12
5162440-16244098.66899.75
6159809-15980997.07098.09
30min1159487-15948796.87598.901.4998.51100.511.52
2163495-16349599.309100.85
3161964-16196498.37999.96
4166822-166822101.330103.10
5163176-16317699.115100.74
6161941-16194198.36599.92
45min1164596-16459699.978100.051.43102.15102.221.46
2165615-165615100.597102.69
3165258-165258100.380102.51
4168135-168135102.127104.46
5163635-16363599.394101.57
6161018-16101897.80499.91
60min1165623-165623100.60299.571.37103.33102.301.34
2167101-167101101.499104.15
3160817-16081797.682100.37
4164012-16401299.623102.52
5163573-16357399.356102.09
6162437-16243798.666101.31
极限1164013-16401399.62499.461.31102.91102.741.33
2165767-165767100.689103.90
3162396-16239698.641101.87
4166700-166700101.256104.71
5162280-16228098.571101.85
6161333-16133397.996101.19
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2024-07-19 17:22:02 完成)
生成报告数据部分下载报告(谢超君 于 2024-07-19 17:22:21 完成)
Current page cost:58 ms