贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.782966302965152964522965682964842965300.03
29.742962132972292967210.25
单位质量响应值RSD%判断
30320.0430464.170.34数据可信
供试品溶液-24070802批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min119614-1961412.8716.0783.9112.876.0883.91
211338-113387.4407.44
312610-126108.2758.28
4-0.0000.00
511980-119807.8627.86
6-0.0000.00
10min147445-4744531.13527.5812.7631.2827.6512.89
240089-4008926.30726.39
341459-4145927.20727.30
438854-3885425.49725.50
549232-4923232.30732.39
635074-3507423.01623.02
15min171189-7118946.71644.114.6647.2144.494.81
267366-6736644.20744.58
369033-6903345.30145.70
462542-6254241.04241.33
568498-6849844.95045.40
664692-6469242.45342.71
20min185839-8583956.33053.266.4857.3454.126.50
279906-7990652.43653.30
383149-8314954.56555.46
471159-7115946.69647.44
583206-8320654.60255.55
683669-8366954.90655.63
30min199064-9906465.00863.093.7966.6464.553.66
297139-9713963.74565.19
393471-9347161.33862.84
495538-9553862.69563.95
590887-9088759.64261.19
6100770-10077066.12867.47
45min1118935-11893578.04875.512.8380.4077.672.88
2111189-11118972.96575.12
3117655-11765577.20879.39
4111722-11172273.31575.27
5116951-11695176.74678.96
6113959-11395974.78376.86
60min1123565-12356581.08780.821.5384.3183.821.59
2124899-12489981.96284.93
3123925-12392581.32384.37
4119503-11950378.42181.19
5123312-12331280.92183.99
6123756-12375681.21284.12
极限1130566-13056685.68187.463.1289.8191.363.00
2134478-13447888.24892.13
3131559-13155986.33390.28
4127965-12796583.97487.61
5135339-13533988.81392.78
6139765-13976591.71895.52
贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.782973222972882972662975402973082973450.04
29.742953972954442954200.02
单位质量响应值RSD%判断
30403.3730330.600.17数据可信
供试品溶液-24071201批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1-0.0003.03156.630.003.03156.63
2-0.0000.00
3-0.0000.00
4-0.0000.00
512156-121567.9847.98
615516-1551610.19010.19
10min138135-3813525.04633.8913.7325.0533.9313.80
252635-5263534.56934.57
351452-5145233.79233.79
453839-5383935.36035.36
558986-5898638.74038.83
654593-5459335.85535.97
15min168893-6889345.24749.675.1345.5250.085.21
278990-7899051.87852.26
373211-7321148.08348.46
478244-7824451.38851.78
577817-7781751.10851.63
676615-7661550.31850.83
20min186322-8632256.69359.802.9557.4760.763.06
292695-9269560.87961.84
391798-9179860.29061.20
489527-8952758.79859.76
592541-9254160.77861.86
693432-9343261.36362.43
30min198208-9820864.50068.544.5965.9170.164.54
2109306-10930671.78973.43
3105922-10592269.56671.15
4105691-10569169.41471.03
598685-9868564.81366.58
6108300-10830071.12872.88
45min1115853-11585376.08879.052.1278.2281.442.21
2123426-12342681.06283.50
3119840-11984078.70781.06
4120578-12057879.19281.58
5121876-12187680.04482.53
6120622-12062279.22181.76
60min1129666-12966685.16082.353.1988.1385.622.99
2128476-12847684.37987.71
3119371-11937178.39981.63
4127401-12740183.67386.94
5125415-12541582.36885.74
6122007-12200780.13083.55
极限1131517-13151786.37686.762.1890.3090.942.16
2136431-13643189.60393.88
3129717-12971785.19489.29
4129121-12912184.80289.00
5131138-13113886.12790.41
6134722-13472288.48192.79
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