阿齐沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DJ301-191212对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数1000
标示量(mg)20供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.272985352974582989182964002990442980710.38
211.252968142968622968380.02
单位质量响应值RSD%判断
26448.1826385.600.17数据可信
供试品溶液-2023101221批-阿齐沙坦-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19969-99693.3882.9722.313.392.9722.33
26536-65362.2212.22
310098-100983.4323.43
410099-100993.4323.43
59818-98183.3373.34
65947-59472.0212.02
10min119746-197466.7105.799.216.735.809.19
217232-172325.8565.87
317603-176035.9826.00
416408-164085.5765.60
515626-156265.3105.33
615551-155515.2855.30
15min124696-246968.3937.865.238.457.905.27
223391-233917.9497.99
324034-240348.1688.22
423123-231237.8587.91
521525-215257.3157.36
621956-219567.4627.50
20min128616-286169.7259.283.979.839.383.98
227757-277579.4339.52
328052-280529.5339.63
427457-274579.3319.42
525860-258608.7888.88
626174-261748.8958.98
30min133358-3335811.33611.211.7711.4911.351.80
233017-3301711.22011.36
333368-3336811.34011.49
433564-3356411.40611.55
532028-3202810.88411.02
632599-3259911.07811.21
45min138178-3817812.97412.722.6013.1912.932.61
237618-3761812.78412.99
338259-3825913.00213.22
437957-3795712.89913.11
535744-3574412.14712.35
636854-3685412.52412.72
60min140669-4066913.82113.512.1214.1113.792.15
240405-4040513.73114.01
340207-4020713.66413.95
439677-3967713.48413.76
538476-3847613.07613.34
639094-3909413.28613.55
极限142001-4200114.27414.051.8414.6414.401.88
241713-4171314.17614.53
342225-4222514.35014.71
441109-4110913.97014.33
540332-4033213.70614.04
640685-4068513.82614.16
阿齐沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DJ301-191212对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数1000
标示量(mg)20供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.272960182960922959872959562959832960070.02
211.252962352978502970420.39
单位质量响应值RSD%判断
26265.0426403.730.38数据可信
供试品溶液-2023101221批-阿齐沙坦-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17153-71532.4394.3855.162.444.3855.15
215886-158865.4165.42
37454-74542.5412.54
46480-64802.2092.21
515842-158425.4015.40
624291-242918.2818.28
10min113388-133884.5645.369.414.585.389.40
215710-157105.3565.39
316805-168055.7295.74
416748-167485.7105.72
514572-145724.9685.00
617110-171105.8335.88
15min120042-200426.8327.495.946.877.545.95
221910-219107.4697.53
323100-231007.8757.92
423056-230567.8607.90
520770-207707.0817.14
622900-229007.8077.89
20min124905-249058.4908.943.898.579.043.90
226238-262388.9459.05
326986-269869.2009.29
427369-273699.3309.42
525093-250938.5548.65
626736-267369.1149.24
30min130604-3060410.43310.852.9310.5611.002.96
232030-3203010.91911.07
332541-3254111.09311.23
432705-3270511.14911.29
530736-3073610.47810.62
632399-3239911.04511.22
45min135301-3530112.03412.451.9112.2212.661.97
236625-3662512.48612.70
337016-3701612.61912.82
437094-3709412.64612.85
536166-3616612.32912.53
636996-3699612.61212.85
60min138949-3894913.27813.471.4613.5313.741.50
239226-3922613.37213.65
338976-3897613.28713.56
439454-3945413.45013.72
540166-4016613.69313.96
640245-4024513.72014.02
极限139779-3977913.56113.871.1413.8814.221.20
240867-4086713.93214.29
340778-4077813.90114.25
440940-4094013.95714.30
541055-4105513.99614.34
640706-4070613.87714.26
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