苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263777537971378283810437914379180.34
213.303787037879378740.02
单位质量响应值RSD%判断
2859.582847.670.30数据可信
供试品溶液-8153342批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127692-2769261.27062.365.7461.2762.365.74
225128-2512855.59755.60
328947-2894764.04764.05
429248-2924864.71364.71
528663-2866363.41963.42
629432-2943265.12065.12
10min135447-3544778.42980.875.5079.1181.565.50
232940-3294072.88273.50
337250-3725082.41883.13
437672-3767283.35284.07
537964-3796483.99884.70
638034-3803484.15384.88
15min138375-3837584.90786.095.0886.4687.695.08
235399-3539978.32379.75
338846-3884685.94987.58
439471-3947187.33288.98
540370-4037089.32190.96
641010-4101090.73792.40
20min139672-3967287.77788.644.4190.2791.184.43
236736-3673681.28183.58
340688-4068890.02592.61
440467-4046789.53692.15
541071-4107190.87293.50
641732-4173292.33595.00
30min142006-4200692.94192.474.5796.4196.014.57
238203-3820384.52787.73
341946-4194692.80896.39
441951-4195192.81996.43
543822-4382296.959100.60
642841-4284194.78898.48
45min141967-4196792.85592.273.5997.3696.833.65
238843-3884385.94390.08
342248-4224893.47698.09
441518-4151891.86196.50
542565-4256594.17898.90
643068-4306895.291100.04
极限142927-4292794.97994.792.68100.51100.372.78
240587-4058789.80194.90
343540-4354096.335101.99
442912-4291294.946100.61
543470-4347096.180101.94
643608-4360896.485102.29
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263781937963378693792137864378870.15
213.303796437680378220.54
单位质量响应值RSD%判断
2857.242843.760.34数据可信
供试品溶液-8153342批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min129962-2996266.36663.715.0666.3763.725.06
229610-2961065.58665.59
329255-2925564.80064.80
429556-2955665.46665.47
528104-2810462.25062.25
626099-2609957.80957.81
10min137614-3761483.31583.392.2784.0584.102.28
237608-3760883.30184.03
337526-3752683.12083.84
439177-3917786.77787.50
537413-3741382.86983.56
636544-3654480.94581.59
15min139872-3987288.31688.982.3589.9890.612.36
240185-4018589.00990.66
340132-4013288.89290.54
441975-4197592.97494.67
539477-3947787.44189.05
639379-3937987.22488.77
20min140619-4061989.97190.481.7592.6293.111.77
240791-4079190.35293.00
340784-4078490.33692.97
442110-4211093.27396.00
540896-4089690.58493.17
639904-3990488.38790.90
30min140655-4065590.05092.362.9793.6995.982.93
241338-4133891.56395.21
342089-4208993.22796.86
444014-4401497.491101.25
541148-4114891.14294.73
640930-4093090.66094.15
45min142079-4207993.20593.091.1497.8597.751.13
242000-4200093.03097.69
342425-4242593.97198.64
442370-4237093.84998.69
541112-4111291.06395.67
642183-4218393.43597.94
极限142632-4263294.43095.652.07100.11101.341.96
244870-4487099.387105.08
343485-4348596.319102.03
442788-4278894.775100.66
542559-4255994.26899.88
642770-4277094.735100.27
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263786837910376343807438040379050.47
213.303808137954380180.24
单位质量响应值RSD%判断
2858.602858.500.01数据可信
供试品溶液-8153342批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min145798-45798101.156102.362.41101.16102.362.42
245274-4527499.999100.00
348112-48112106.267106.27
447103-47103104.038104.04
545307-45307100.072100.07
646476-46476102.654102.65
10min147009-47009103.831101.502.21104.95102.642.20
245537-45537100.580101.69
346667-46667103.075104.26
446666-46666103.073104.23
544334-4433497.92299.03
645520-45520100.542101.68
15min145680-45680100.895100.232.76103.17102.502.74
245356-45356100.180102.41
347242-47242104.345106.67
445897-45897101.375103.68
543590-4359096.27998.48
644508-4450898.307100.56
20min145457-45457100.40399.402.00103.80102.782.00
244520-4452098.333101.68
346523-46523102.757106.24
444977-4497799.343102.77
543945-4394597.063100.33
644605-4460598.521101.87
30min144846-4484699.05398.232.20103.57102.722.19
244337-4433797.929102.36
345528-45528100.560105.19
445015-4501599.427103.96
542686-4268694.28298.63
644429-4442998.132102.58
45min144613-4461398.53997.481.97104.15103.061.98
243733-4373396.595102.12
345124-4512499.667105.41
444716-4471698.766104.40
542719-4271994.35599.75
643904-4390496.973102.51
极限144050-4405097.29596.102.46104.00102.762.43
242939-4293994.841101.44
345069-4506999.546106.40
443528-4352896.142102.88
541876-4187692.49398.94
643585-4358596.268102.88
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263793837939379453813737882379680.26
213.303789338080379860.35
单位质量响应值RSD%判断
2863.352856.090.18数据可信
供试品溶液-8153342批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144157-4415797.49299.172.4297.4999.162.42
244922-4492299.18199.18
346599-46599102.883102.88
445181-4518199.75299.75
545237-4523799.87699.88
643397-4339795.81495.81
10min144248-4424897.693101.002.4698.78102.102.46
245677-45677100.848101.95
347289-47289104.407105.55
446429-46429102.508103.62
546110-46110101.804102.91
644713-4471398.71999.78
15min144860-4486099.044100.801.83101.21103.021.84
246170-46170101.936104.16
346543-46543102.760105.06
446167-46167101.929104.18
545765-45765101.042103.28
644425-4442598.083100.24
20min143614-4361496.29398.912.2199.56102.252.20
245542-45542100.550103.90
345990-45990101.539104.98
444918-4491899.172102.55
545102-4510299.578102.94
643623-4362396.31399.56
30min143836-4383696.78398.382.43101.12102.822.42
244802-4480298.916103.39
346250-46250102.113106.69
444970-4497099.287103.77
544421-4442198.075102.54
643071-4307195.09499.42
45min142706-4270694.28897.862.5199.70103.392.48
244331-4433197.876103.45
346040-46040101.649107.36
444206-4420697.600103.18
544864-4486499.053104.61
643791-4379196.684102.06
极限142174-4217493.11497.083.0199.58103.712.95
243861-4386196.838103.50
346133-46133101.854108.69
444286-4428697.776104.45
544209-4420997.606104.27
643173-4317395.319101.77
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