苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263744337439374593739937317374110.16
213.303731737217372670.19
单位质量响应值RSD%判断
2821.342802.030.49数据可信
供试品溶液-8165511批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125383-2538357.00057.534.1257.0057.534.12
227303-2730361.31161.31
324619-2461955.28455.28
426510-2651059.53059.53
524953-2495356.03456.03
624959-2495956.04756.05
10min139620-3962088.97090.051.7189.6090.681.72
240686-4068691.36492.04
339269-3926988.18288.80
441069-4106992.22492.89
539747-3974789.25589.88
640204-4020490.28190.90
15min141312-4131292.76994.151.8494.3995.791.83
241289-4128992.71894.41
341277-4127792.69194.28
443120-4312096.82998.52
542074-4207494.48196.09
642494-4249495.42497.05
20min141978-4197894.26594.941.1896.9297.621.14
241770-4177093.79896.52
342078-4207894.49097.11
442356-4235695.11497.88
543190-4319096.98799.65
642290-4229094.96697.65
30min142779-4277996.06495.462.0599.7699.201.96
242000-4200094.31498.08
341634-4163493.49397.17
441738-4173893.72697.54
543819-4381998.399102.14
643104-4310496.794100.53
45min143144-4314496.88395.461.93101.65100.261.84
242135-4213594.61899.43
342063-4206394.45699.17
442042-4204294.40999.27
543880-4388098.536103.37
641807-4180793.88198.70
极限142858-4285896.24194.911.86102.09100.781.79
241559-4155993.32499.19
341412-4141292.99498.76
442393-4239395.197101.11
543437-4343797.541103.47
641941-4194194.182100.04
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263731237329372743713037282372650.22
213.303749937457374780.08
单位质量响应值RSD%判断
2810.332817.890.19数据可信
供试品溶液-8165511批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min132645-3264573.24374.573.8673.2474.573.86
231963-3196371.71371.71
334302-3430276.96176.96
434795-3479578.06778.07
531770-3177071.28071.28
633948-3394876.16776.17
10min140105-4010589.98091.353.8090.7992.183.79
241275-4127592.60693.40
342352-4235295.02295.88
441948-4194894.11594.98
538068-3806885.41086.20
640545-4054590.96891.81
15min141072-4107292.15093.573.3193.9695.423.30
242983-4298396.43898.26
342680-4268095.75897.67
442689-4268995.77897.69
539359-3935988.30790.05
641452-4145293.00394.86
20min140735-4073591.39494.012.9894.2396.892.98
242708-4270895.82198.72
342761-4276195.94098.91
442768-4276895.95598.93
539924-3992489.57492.30
642510-4251095.37698.27
30min140616-4061691.12793.242.4094.9897.172.42
242436-4243695.21099.17
342330-4233094.97399.01
441787-4178793.75497.80
540037-4003789.82893.55
642135-4213594.53598.49
45min141039-4103992.07692.442.5596.9497.412.56
242042-4204294.32699.35
341540-4154093.20098.30
441814-4181493.81598.90
539173-3917387.88992.60
641608-4160893.35398.35
极限140034-4003489.82191.522.8195.7197.512.81
241640-4164093.42499.49
341267-4126792.58898.72
441514-4151493.14299.27
538787-3878787.02392.72
641496-4149693.10199.14
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263729137285373733721437329372980.16
213.303697636999369880.05
单位质量响应值RSD%判断
2812.822781.050.81数据可信
供试品溶液-8165511批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min132693-3269373.80372.464.5573.8072.464.55
234533-3453377.95777.96
331066-3106670.13170.13
432474-3247473.30973.31
531323-3132370.71170.71
630505-3050568.86468.86
10min136702-3670282.85483.244.5483.6784.054.53
239376-3937688.89089.76
335464-3546480.05980.84
436500-3650082.39883.21
538247-3824786.34187.13
634951-3495178.90179.67
15min138195-3819586.22486.133.5787.9687.863.59
240344-4034491.07592.93
336852-3685283.19284.86
437971-3797185.71887.45
538894-3889487.80289.55
636672-3667282.78684.43
20min138367-3836786.61286.563.3589.3189.253.36
240008-4000890.31793.18
336649-3664982.73485.33
437973-3797385.72388.41
539622-3962289.44592.17
637438-3743884.51587.08
30min139312-3931288.74688.472.1692.4192.122.21
240237-4023790.83494.70
338025-3802585.84089.35
438857-3885787.71991.35
540034-4003490.37694.09
638669-3866987.29490.79
45min139395-3939588.93389.331.4693.5893.961.51
240096-4009690.51695.39
338565-3856587.05991.53
439529-3952989.23693.85
540138-4013890.61095.33
639690-3969089.59994.07
极限140910-4091092.35393.890.9497.9999.520.88
241650-4165094.02499.91
341791-4179194.34299.78
441395-4139593.44899.05
541966-4196694.737100.46
641841-4184194.45599.92
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数4系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.263717537183372193719137264372060.10
213.303733937217372780.24
单位质量响应值RSD%判断
2805.882802.860.08数据可信
供试品溶液-8165511批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min130928-3092869.63274.343.5569.6374.343.55
233512-3351275.44975.45
333813-3381376.12776.13
434189-3418976.97476.97
532552-3255273.28873.29
633123-3312374.57474.57
10min135010-3501078.82284.274.2079.6085.104.19
237381-3738184.16085.00
339275-3927588.42489.27
438927-3892787.64188.50
536532-3653282.24983.06
637449-3744984.31385.14
15min136484-3648482.14186.783.8283.7988.543.81
238545-3854586.78188.55
340548-4054891.29093.12
439838-3983889.69291.52
537705-3770584.89086.62
638155-3815585.90387.67
20min137070-3707083.46086.432.3986.0289.162.37
238908-3890887.59890.34
337478-3747884.37987.22
439423-3942388.75891.58
538574-3857486.84689.52
638881-3888187.53790.26
30min137604-3760484.66288.823.2488.1592.503.22
239491-3949188.91192.62
341223-4122392.81096.59
439922-3992289.88193.69
538430-3843086.52290.16
640021-4002190.10493.80
45min138344-3834486.32889.723.0590.7694.393.04
239350-3935088.59393.29
341426-4142693.26798.08
441052-4105292.42597.24
538904-3890487.58992.19
640014-4001490.08894.78
极限139397-3939788.69993.443.6194.0999.113.56
241076-4107692.47998.16
342308-4230895.253101.10
442727-4272796.196102.03
540281-4028190.68996.26
643223-4322397.313103.01
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