盐酸司来吉兰片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号101298-201801对照品来源中检院对照品使用方法减压干燥3h
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.944389294389144387744384454388024387730.05
210.014377924378554378240.02
单位质量响应值RSD%判断
44142.1543738.660.65数据可信
供试品溶液-24072401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1226327-22632751.25155.2822.7751.2555.2822.77
2309412-30941270.06670.07
3185616-18561642.03242.03
4177812-17781240.26540.27
5288143-28814365.24965.25
6277466-27746662.83262.83
10min1305313-30531369.13776.2814.2569.2976.4514.27
2391714-39171488.70388.91
3303045-30304568.62468.75
4279413-27941363.27263.39
5351462-35146279.58879.78
6390277-39027788.37788.57
15min1332418-33241875.27581.3610.6475.6481.7510.67
2404059-40405991.49891.97
3336270-33627076.14876.48
4313472-31347270.98571.30
5366673-36667383.03283.47
6402764-40276491.20591.66
20min1345833-34583378.31383.648.3278.9084.288.37
2405087-40508791.73192.48
3348350-34835078.88379.44
4335989-33598976.08476.61
5375457-37545785.02185.71
6405314-40531491.78292.51
30min1360638-36063881.66686.536.3982.4987.426.46
2412499-41249993.41094.44
3365519-36551982.77183.57
4358197-35819781.11381.86
5386754-38675487.58088.52
6409043-40904392.62793.63
45min1372722-37272284.40288.924.5385.4790.074.62
2415418-41541894.07195.38
3383391-38339186.81887.86
4376983-37698385.36786.36
5397212-39721289.94891.15
6410368-41036892.92794.21
60min1380779-38077986.22790.173.7987.5591.593.88
2418136-41813694.68696.27
3388427-38842787.95889.26
4386671-38667187.56188.81
5404003-40400391.48692.96
6411246-41124693.12694.69
极限1418383-41838394.74295.831.8896.3297.521.92
2432881-43288198.02599.90
3423097-42309795.80997.38
4417226-41722694.48095.99
5432752-43275297.99699.74
6414738-41473893.91795.76
盐酸司来吉兰片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号101298-201801对照品来源中检院对照品使用方法减压干燥3h
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.944380204381364378534378694379554379670.03
210.014354314352644353480.03
单位质量响应值RSD%判断
44061.0743491.310.93数据可信
供试品溶液-24072402批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1302738-30273868.81350.9918.9568.8150.9918.95
2212164-21216448.22548.23
3217239-21723949.37949.38
4184093-18409341.84541.84
5236013-23601353.64653.65
6193809-19380944.05344.05
10min1357961-35796181.36563.4814.6781.5763.6314.68
2282869-28286964.29764.44
3250718-25071856.98957.14
4259615-25961559.01159.14
5276475-27647562.84363.00
6248018-24801856.37556.51
15min1368074-36807483.66467.9313.0784.1168.2713.08
2316917-31691772.03672.37
3266790-26679060.64260.96
4280289-28028963.71064.01
5295702-29570267.21467.56
6265306-26530660.30560.61
20min1375237-37523785.29270.8911.9285.9971.4411.94
2333548-33354875.81676.37
3281037-28103763.88064.38
4294609-29460966.96567.46
5308996-30899670.23570.79
6277786-27778663.14163.62
30min1382361-38236186.91174.819.6787.8775.569.71
2348468-34846879.20879.99
3300309-30030968.26168.95
4315497-31549771.71372.41
5327715-32771574.49075.25
6300258-30025868.24968.92
45min1396305-39630590.08179.247.9691.3080.228.02
2364142-36414282.77083.79
3326453-32645374.20375.10
4337568-33756876.73077.64
5345106-34510678.44379.43
6321994-32199473.19074.07
60min1404082-40408291.84981.947.0193.3483.167.08
2374349-37434985.09086.36
3343941-34394178.17979.30
4351679-35167979.93781.08
5355255-35525580.75081.97
6333673-33367375.84576.94
极限1419860-41986095.43593.351.3697.2094.821.48
2412120-41212093.67695.20
3412902-41290293.85495.21
4408513-40851392.85694.24
5406351-40635192.36493.83
6404387-40438791.91893.24
点击查看处理图标(自动生成)
　
原始图谱下载图谱(刘齐慧子 于 2024-07-29 18:29:32 完成)
生成报告数据部分(等待生成报告)
Current page cost:54 ms