恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DC033-12306002对照品来源分装对照品使用方法直接使用
对照品含量(%)98.99对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.292859001285963528594112859403285985728594610.02
210.352856476285533728559060.03
单位质量响应值RSD%判断
277887.37275932.950.50数据可信
每杯投5片--供试品溶液-2024052811批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11942823-194282362.50866.154.8662.5166.154.86
21956728-195672862.95562.96
32154871-215487169.33069.33
42128324-212832468.47668.48
52001763-200176364.40464.40
62151943-215194369.23669.24
10min12459432-245943279.12981.422.7879.2381.532.78
22465939-246593979.33879.44
32614671-261467184.12484.24
42533933-253393381.52681.64
52495182-249518280.27980.39
62614407-261440784.11584.23
15min12611609-261160984.02585.352.0884.2685.602.09
22603049-260304983.75083.99
32725279-272527987.68287.94
42633684-263368484.73584.99
52623043-262304384.39384.63
62720212-272021287.51987.77
20min12650563-265056385.27886.531.9085.6586.921.90
22644258-264425885.07585.45
32754111-275411188.61089.01
42671326-267132685.94686.34
52662308-266230885.65686.04
62754167-275416788.61289.01
30min12680116-268011686.22987.301.7886.7587.841.78
22673619-267361986.02086.54
32771666-277166689.17589.72
42690037-269003786.54887.08
52687187-268718786.45786.98
62778455-277845589.39389.94
45min12701824-270182486.92887.831.6687.5988.511.66
22689658-268965886.53687.20
32780587-278058789.46290.16
42713649-271364987.30887.99
52700442-270044286.88387.55
62793792-279379289.88690.58
60min12705764-270576487.05487.931.7387.8688.761.73
22696337-269633786.75187.56
32783368-278336889.55190.40
42702910-270291086.96287.79
52706921-270692187.09287.90
62802673-280267390.17291.02
极限13043814-304381497.93198.142.0598.8899.112.05
23018528-301852897.11798.07
33067745-306774598.70199.70
42976027-297602795.75096.72
53034229-303422997.62298.58
63161764-3161764101.725102.72
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