替米沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数1250
标示量(mg)80供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.037478017478937476127473137469027475040.06
211.097434137435717434920.02
单位质量响应值RSD%判断
67770.0867041.660.77数据可信
供试品溶液-2023052121批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1167790-16779022.40423.546.0022.4023.546.00
2176543-17654323.57323.57
3192483-19248325.70125.70
4180014-18001424.03624.04
5162036-16203621.63621.64
6178886-17888623.88523.89
10min1353447-35344747.19347.9710.2447.3248.1010.23
2354923-35492347.39147.52
3418175-41817555.83655.98
4357942-35794247.79447.93
5303078-30307840.46840.59
6368173-36817349.16049.29
15min1477025-47702563.69464.2511.1764.0864.6511.15
2479384-47938464.00964.40
3563041-56304175.17975.63
4464502-46450262.02262.42
5398284-39828453.18053.53
6505024-50502467.43367.84
20min1558090-55809074.51875.4211.0775.2676.1811.06
2567511-56751175.77676.53
3665882-66588288.91189.78
4543999-54399972.63773.38
5472258-47225863.05863.70
6581401-58140177.63178.41
30min1636980-63698085.05285.968.1486.2187.148.17
2661010-66101088.26089.43
3727114-72711497.08798.45
4636545-63654584.99486.14
5564170-56417075.33076.32
6637023-63702385.05786.27
45min1713472-71347295.26594.984.9896.8996.635.05
2719165-71916596.02597.69
3766672-766672102.369104.27
4703387-70338793.91995.54
5656037-65603787.59689.01
6709165-70916594.69096.37
60min1715283-71528395.50796.813.4497.6698.993.54
2729886-72988697.45799.65
3761280-761280101.649104.12
4733242-73324297.905100.05
5684994-68499491.46393.36
6725606-72560696.88599.10
极限1585020-58502078.11484.084.9780.8086.794.94
2613736-61373681.94884.68
3679415-67941590.71893.76
4642315-64231585.76488.45
5629851-62985184.10086.50
6627723-62772383.81686.56
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