贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.68 2923662925532924732924282923312924300.04
29.66 2917872919712918790.05
单位质量响应值RSD%判断
30209.7130215.220.02数据可信
供试品溶液-24072201批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min194735-9473531.26832.048.6331.2732.048.63
2104026-10402634.33534.34
3101786-10178633.59633.60
4104280-10428034.41934.42
595355-9535531.47331.47
682255-8225527.14927.15
10min1239813-23981379.15379.372.3679.2179.422.37
2245881-24588181.15681.21
3242391-24239180.00480.06
4243982-24398280.52980.59
5240906-24090679.51479.57
6229770-22977075.83875.88
15min1281203-28120392.81593.200.8593.0093.390.85
2282973-28297393.39993.59
3282734-28273493.32093.51
4284815-28481594.00794.20
5284284-28428493.83194.02
6278282-27828291.85092.02
20min1293796-29379696.97197.400.6997.3197.740.69
2294519-29451997.21097.56
3294859-29485997.32297.67
4296809-29680997.96698.31
5298058-29805898.37898.72
6292530-29253096.55396.88
30min1302124-30212499.72099.770.77100.22100.270.77
2300955-30095599.33499.84
3301743-30174399.594100.10
4302782-30278299.937100.45
5306456-306456101.150101.65
6299582-29958298.88199.37
45min1303539-303539100.18784.6645.88100.8585.3345.52
216345-163455.3956.07
3304132-304132100.383101.06
4304475-304475100.496101.17
5307955-307955101.644102.32
6302536-30253699.856100.51
60min1304525-304525100.512100.901.31101.35101.721.33
2302828-30282899.952100.64
3304526-304526100.513101.35
4304482-304482100.498101.34
5313765-313765103.562104.41
6304137-304137100.384101.20
极限1304669-304669100.560100.810.59101.56101.790.64
2302673-30267399.901100.75
3305864-305864100.954101.96
4304896-304896100.635101.65
5307949-307949101.642102.66
6306515-306515101.169102.15
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