坎地沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.334249642261424244243742080423400.40
214.364219142246422180.10
单位质量响应值RSD%判断
2954.642939.970.36数据可信
供试品溶液-2024042711批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min148350-48350103.57796.376.79103.5896.376.79
244215-4421594.71994.72
339987-3998785.66285.66
447913-47913102.641102.64
544031-4403194.32594.32
645419-4541997.29897.30
10min148229-48229103.318101.982.42104.47103.052.46
248225-48225103.309104.36
345748-4574898.00398.95
448946-48946104.854105.99
546829-46829100.319101.37
647654-47654102.086103.17
15min147917-47917102.650101.891.67104.95104.091.69
248482-48482103.860106.06
346984-46984100.651102.69
448354-48354103.586105.89
546630-4663099.893102.06
646999-46999100.683102.90
20min147274-47274101.272101.221.29104.71104.561.29
247483-47483101.720105.07
347442-47442101.632104.79
448072-48072102.982106.44
546259-4625999.098102.37
646968-46968100.617103.95
30min145962-4596298.46299.401.49103.03103.861.47
246961-46961100.602105.09
346627-4662799.886104.17
447281-47281101.287105.89
545405-4540597.268101.64
646154-4615498.873103.32
45min145546-4554697.57097.991.37103.23103.551.36
245878-4587898.282103.88
346015-4601598.575103.97
446657-4665799.950105.68
544774-4477495.917101.37
645569-4556997.620103.17
60min145117-4511796.65196.682.75103.39103.342.63
245173-4517396.771103.47
346244-4624499.066105.56
446266-4626699.113105.95
542857-4285791.81098.33
645131-4513196.681103.32
极限144609-4460995.56395.901.07103.38103.631.10
245331-4533197.110104.88
344709-4470995.777103.37
445237-4523796.908104.85
544023-4402394.308101.85
644684-4468495.724103.43
坎地沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.334233542352422924237842347423410.08
214.364235642177422660.30
单位质量响应值RSD%判断
2954.712943.310.28数据可信
供试品溶液-2024042711批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min147275-47275101.21699.303.47101.2299.303.47
247021-47021100.672100.67
347404-47404101.492101.49
446388-4638899.31699.32
543175-4317592.43792.44
647024-47024100.678100.68
10min148158-48158103.106102.071.63104.23103.181.65
247604-47604101.920103.04
347496-47496101.689102.82
448057-48057102.890103.99
546271-4627199.066100.09
648468-48468103.770104.89
15min146911-46911100.436101.231.36102.71103.461.36
247413-47413101.511103.76
346789-46789100.175102.43
448019-48019102.808105.06
546525-4652599.610101.74
648024-48024102.819105.09
20min146819-46819100.239100.020.87103.63103.380.87
246234-4623498.987102.37
346455-4645599.460102.83
447227-47227101.113104.50
546430-4643099.406102.64
647122-47122100.888104.30
30min146719-46719100.02599.161.70104.53103.641.69
246063-4606398.621103.10
345696-4569697.835102.31
447095-47095100.830105.34
545210-4521096.794101.13
647114-47114100.871105.41
45min146227-4622798.97298.251.18104.58103.821.16
245389-4538997.178102.75
345380-4538097.158102.72
446755-46755100.102105.74
545631-4563197.696103.11
645953-4595398.385104.04
60min145636-4563697.70696.560.90104.42103.230.88
245240-4524096.859103.51
344657-4465795.610102.25
445457-4545797.323104.07
544863-4486396.051102.55
644750-4475095.810102.56
极限144454-4445495.17695.440.84102.97103.180.85
244427-4442795.118102.85
344278-4427894.799102.50
445182-4518296.734104.56
544251-4425194.741102.31
644884-4488496.096103.91
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