枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.604658504657314656474654634656844656750.04
217.634635864642294639080.10
单位质量响应值RSD%判断
26458.8126313.560.39数据可信
供试品溶液-50124002批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1384434-38443473.77372.982.0073.7772.982.00
2378862-37886272.70372.70
3386458-38645874.16174.16
4366817-36681770.39270.39
5378306-37830672.59772.60
6387043-38704374.27374.27
10min1391091-39109175.05074.511.1475.1774.631.14
2382532-38253273.40873.53
3391772-39177275.18175.30
4383323-38332373.56073.68
5388261-38826174.50774.63
6392700-39270075.35975.48
15min1387137-38713774.29174.060.9674.5474.300.96
2383678-38367873.62873.87
3388975-38897574.64474.89
4379872-37987272.89773.14
5386092-38609274.09174.34
6389782-38978274.79975.05
20min1386861-38686174.23873.272.0174.6173.642.00
2381091-38109173.13173.50
3386495-38649574.16874.54
4379089-37908972.74773.11
5368197-36819770.65771.03
6389090-38909074.66675.04
30min1383568-38356873.60773.091.0374.1073.581.03
2376616-37661672.27272.76
3382591-38259173.41973.92
4375960-37596072.14772.63
5380668-38066873.05073.54
6385730-38573074.02174.52
45min1380157-38015772.95272.301.1973.5772.911.19
2371714-37171471.33271.94
3379296-37929672.78773.41
4371019-37101971.19871.80
5376763-37676372.30172.91
6381544-38154473.21873.84
极限1373645-37364571.70271.000.9072.4471.740.90
2366843-36684370.39771.12
3370063-37006371.01571.76
4365920-36592070.22070.94
5369770-36977070.95971.69
6373782-37378271.72972.47
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