枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.604685644688624688494691904691764689280.06
217.634714574709134711850.09
单位质量响应值RSD%判断
26643.6426726.320.22数据可信
供试品溶液-50124001批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1378415-37841571.80473.511.5171.8073.501.51
2390135-39013574.02874.03
3390307-39030774.06174.06
4394426-39442674.84274.84
5388454-38845473.70973.71
6382562-38256272.59172.59
10min1385109-38510973.07474.621.1873.1974.741.18
2398251-39825175.56875.69
3393784-39378474.72074.84
4396783-39678375.29075.41
5393606-39360674.68774.81
6391920-39192074.36774.49
15min1385029-38502973.05974.261.0173.3074.511.01
2394756-39475674.90575.15
3391500-39150074.28774.54
4396184-39618475.17675.43
5390813-39081374.15774.40
6389889-38988973.98174.23
20min1381568-38156872.40373.941.2072.7774.311.20
2392549-39254974.48674.86
3388877-38887773.78974.16
4395381-39538175.02475.40
5388930-38893073.79974.17
6390620-39062074.12074.49
30min1377638-37763871.65773.211.3572.1473.711.35
2388032-38803273.62974.13
3382881-38288172.65273.15
4393085-39308574.58875.09
5386468-38646873.33273.83
6386913-38691373.41773.91
45min1374285-37428571.02172.521.2171.6273.131.21
2385547-38554773.15873.78
3381460-38146072.38273.00
4387822-38782273.58974.21
5381920-38192072.46973.09
6382012-38201272.48773.10
极限1369670-36967070.14571.160.9070.8771.900.90
2375796-37579671.30772.05
3375498-37549871.25171.99
4380129-38012972.12972.88
5374033-37403370.97371.71
6375074-37507471.17071.91
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.604693984685884690314693614699624692680.11
217.634705934706454706190.01
单位质量响应值RSD%判断
26662.9526694.210.09数据可信
供试品溶液-50124003批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1385685-38568573.20173.051.2573.2073.051.25
2392320-39232074.46074.46
3380121-38012172.14572.15
4386760-38676073.40573.41
5379152-37915271.96171.96
6385316-38531673.13173.13
10min1391201-39120174.24873.990.9274.3774.120.92
2396050-39605075.16875.29
3387913-38791373.62473.74
4389891-38989173.99974.12
5385551-38555173.17673.30
6388550-38855073.74573.87
15min1387564-38756473.55873.421.1573.8073.671.15
2393877-39387774.75675.01
3381032-38103272.31872.56
4387889-38788973.61973.87
5383322-38332272.75372.99
6387449-38744973.53673.78
20min1386971-38697173.44573.041.0073.8173.411.00
2390883-39088374.18874.56
3381023-38102372.31672.68
4382281-38228172.55572.92
5381762-38176272.45772.82
6386138-38613873.28773.65
30min1383522-38352272.79172.660.8573.2873.150.85
2388603-38860373.75574.25
3381096-38109672.33072.81
4382020-38202072.50572.99
5378996-37899671.93272.42
6382808-38280872.65573.14
45min1378821-37882171.89871.810.7872.5172.420.78
2382793-38279372.65273.27
3378303-37830371.80072.40
4374068-37406870.99671.61
5376547-37654771.46772.07
6379632-37963272.05272.66
极限1375198-37519871.21171.020.7771.9471.750.77
2378638-37863871.86472.61
3371189-37118970.45071.17
4374356-37435671.05171.78
5370927-37092770.40071.12
6374812-37481271.13771.87
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