坎地沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.334429144320442474425244268442760.07
214.364441844301443600.19
单位质量响应值RSD%判断
3089.743089.140.02数据可信
供试品溶液-2024042711批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min142588-4258887.03696.945.9387.0496.945.92
245900-4590093.80493.80
349862-49862101.902101.90
449649-49649101.466101.47
549102-49102100.348100.35
647492-4749297.05897.06
10min147615-4761597.309100.492.2898.28101.562.30
249484-49484101.129102.17
349042-49042100.226101.36
449305-49305100.763101.89
551005-51005104.237105.35
648567-4856799.255100.33
15min148757-4875799.64399.341.42101.69101.541.40
248673-4867399.472101.64
348740-4874099.609101.85
448143-4814398.388100.64
549695-49695101.560103.83
647654-4765497.38999.57
20min148537-4853799.19498.731.17102.35102.031.14
248147-4814798.397101.67
348559-4855999.239102.59
447318-4731896.702100.04
548979-48979100.097103.50
648321-4832198.752102.02
30min147696-4769697.47597.011.06101.73101.401.05
247619-4761997.318101.68
347434-4743496.939101.39
447214-4721496.490100.90
548167-4816798.437102.95
646677-4667795.39299.75
45min147698-4769897.47995.901.79102.82101.371.72
246610-4661095.256100.70
346369-4636994.763100.30
446288-4628894.597100.08
548250-4825098.607104.21
646328-4632894.679100.10
60min146075-4607594.16294.920.68100.59101.460.71
246395-4639594.816101.32
346548-4654895.129101.71
446828-4682895.701102.24
546720-4672095.480102.18
646109-4610994.232100.70
极限145646-4564693.28592.821.22100.76100.411.19
245647-4564793.287100.85
345480-4548092.946100.59
444938-4493891.83899.44
546164-4616494.344102.11
644624-4462491.19798.72
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