枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362385922384802386262383512379432383980.12
217.312383272383432383350.01
单位质量响应值RSD%判断
13732.6013768.630.19数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1271973-271973100.150100.012.09100.15100.012.08
2263208-26320896.92396.92
3274933-274933101.240101.24
4267513-26751398.50898.51
5279371-279371102.874102.87
6272554-272554100.364100.36
10min1274687-274687101.150100.352.30101.32100.522.30
2264635-26463597.44897.61
3276775-276775101.918102.09
4270149-27014999.47999.64
5281441-281441103.637103.81
6267429-26742998.47798.64
15min1274122-274122100.942100.052.33101.28100.392.33
2263871-26387197.16797.49
3276045-276045101.650101.99
4269818-26981899.35799.69
5280432-280432103.265103.61
6265930-26593097.92598.26
20min1273424-273424100.68499.682.49101.19100.182.49
2263653-26365397.08697.57
3275790-275790101.556102.06
4268839-26883998.99699.49
5279573-279573102.949103.47
6262867-26286796.79797.29
30min1272633-272633100.39399.532.33101.06100.202.33
2262200-26220096.55197.20
3274917-274917101.234101.91
4268739-26873998.95999.62
5278651-278651102.609103.30
6264616-26461697.44198.10
45min1271691-271691100.04699.732.09100.89100.562.10
2262040-26204096.49397.30
3274048-274048100.914101.76
4268060-26806098.70999.53
5278810-278810102.668103.53
6270289-27028999.530100.35
极限1271085-27108599.82399.302.33100.83100.302.33
2261770-26177096.39397.36
3274407-274407101.046102.06
4268137-26813798.73899.73
5278443-278443102.533103.56
6264183-26418397.28298.27
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362379342377552380652374242376712377700.11
217.312377782380552379160.09
单位质量响应值RSD%判断
13696.4313744.430.25数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1261910-26191096.65798.871.9696.6698.871.96
2267584-26758498.75198.75
3275159-275159101.546101.55
4268016-26801698.91098.91
5262490-26249096.87196.87
6272222-272222100.463100.46
10min1264484-26448497.60799.791.7497.7799.961.74
2271095-271095100.047100.21
3273851-273851101.064101.23
4270976-270976100.003100.17
5265441-26544197.96098.12
6276583-276583102.072102.24
15min1264344-26434497.55599.551.7697.8899.881.76
2270688-27068899.896100.23
3273263-273263100.847101.18
4269985-26998599.63799.97
5264194-26419497.50097.82
6275970-275970101.846102.18
20min1263538-26353897.25899.361.8297.7499.861.82
2270584-27058499.858100.36
3272862-272862100.699101.20
4269296-26929699.38399.88
5263577-26357797.27297.76
6275562-275562101.695102.20
30min1263035-26303597.07299.211.8097.7299.871.80
2269831-26983199.580100.24
3271613-271613100.238100.91
4269353-26935399.404100.07
5263503-26350397.24597.89
6275562-275562101.695102.37
45min1262532-26253296.88798.901.7297.7099.721.72
2269790-26979099.565100.40
3270517-27051799.833100.67
4268462-26846299.07599.90
5262570-26257096.90197.71
6274020-274020101.126101.97
极限1265731-26573198.06799.021.4899.04100.021.48
2269632-26963299.507100.50
3270451-27045199.809100.82
4267995-26799598.90399.90
5262376-26237696.82997.80
6273756-273756101.029102.04
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362381822377872381112380972381862380730.07
217.312379682383002381340.10
单位质量响应值RSD%判断
13713.8813757.020.23数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1273703-273703100.89998.582.04100.9098.582.04
2270383-27038399.67599.67
3264231-26423197.40797.41
4269320-26932099.28399.28
5268649-26864999.03599.04
6258225-25822595.19395.19
10min1278356-278356102.61499.752.10102.7899.912.10
2272496-272496100.454100.62
3266441-26644198.22298.38
4272901-272901100.603100.77
5271340-271340100.027100.19
6262005-26200596.58696.74
15min1278042-278042102.49899.662.17102.84100.002.17
2273328-273328100.760101.09
3265841-26584198.00098.33
4272039-272039100.285100.62
5271413-271413100.054100.39
6261458-26145896.38596.70
20min1276455-276455101.91399.392.07102.4299.882.07
2272357-272357100.402100.90
3265514-26551497.88098.37
4271622-271622100.131100.63
5270913-27091399.870100.37
6260796-26079696.14196.62
30min1276685-276685101.998102.457.36102.68103.117.31
2271335-271335100.026100.69
3318126-318126117.275117.93
4271018-27101899.909100.58
5270363-27036399.667100.33
6259963-25996395.83396.47
45min1276233-276233101.83199.751.32102.68100.591.31
2270916-27091699.871100.71
3265080-26508097.72098.57
4270987-27098799.897100.73
5269869-26986999.485100.32
6270474-27047499.708100.51
极限1275385-275385101.51998.902.28102.5499.902.27
2270675-27067599.782100.78
3263359-26335997.08598.10
4271774-271774100.187101.19
5269740-26974099.438100.43
6258700-25870095.36896.33
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362380762380192384902383752381112382140.09
217.312380292377502378900.09
单位质量响应值RSD%判断
13722.0013742.920.11数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1269419-26941999.34198.371.5299.3498.371.52
2260222-26022295.95095.95
3265074-26507497.73997.74
4265834-26583498.01998.02
5268385-26838598.95998.96
6271782-271782100.212100.21
10min1272705-272705100.552100.212.32100.72100.382.32
2263329-26332997.09597.26
3268080-26808098.84799.01
4269720-26972099.45299.62
5281543-281543103.811103.98
6275344-275344101.525101.69
15min1272128-272128100.34099.511.45100.6799.841.44
2263792-26379297.26697.59
3268031-26803198.82999.16
4269185-26918599.25499.58
5270841-27084199.865100.20
6275240-275240101.487101.82
20min1271980-271980100.28599.331.57100.7999.821.57
2262679-26267996.85697.34
3268136-26813698.86899.36
4268272-26827298.91899.41
5270069-27006999.580100.08
6275174-275174101.463101.97
30min1270968-27096899.91298.931.37100.5899.591.37
2262088-26208896.63897.28
3266957-26695798.43399.09
4267880-26788098.77399.43
5269446-26944699.351100.02
6272504-272504100.478101.15
45min1270292-27029299.66399.370.85100.50100.200.85
2269632-26963299.419100.23
3266829-26682998.38699.21
4267799-26779998.74399.57
5269059-26905999.208100.04
6273394-273394100.806101.65
极限1270325-27032599.67598.901.34100.6799.891.34
2263051-26305196.99397.96
3266309-26630998.19499.18
4267601-26760198.67099.66
5268379-26837998.95799.96
6273632-273632100.894101.90
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362388252386792381812388392380422385130.16
217.312373842375212374520.05
单位质量响应值RSD%判断
13739.2313717.620.12数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1266704-26670498.36999.811.8698.3799.811.86
2278312-278312102.650102.65
3272625-272625100.552100.55
4266214-26621498.18898.19
5266227-26622798.19398.19
6273636-273636100.925100.93
10min1268734-26873499.117101.112.1899.28101.282.18
2283494-283494104.561104.73
3277074-277074102.193102.36
4269108-26910899.25599.42
5269642-26964299.45299.62
6276744-276744102.072102.24
15min1275244-275244101.518101.351.72101.85101.681.72
2281926-281926103.983104.33
3276047-276047101.815102.15
4269259-26925999.31199.64
5269836-26983699.52499.85
6276397-276397101.944102.28
20min1267604-26760498.701100.772.0399.20101.282.03
2282168-282168104.072104.59
3274745-274745101.334101.84
4268784-26878499.13699.63
5269870-26987099.536100.03
6276159-276159101.856102.36
30min1266556-26655698.314100.592.1298.98101.262.12
2281577-281577103.854104.55
3275392-275392101.573102.25
4268232-26823298.93299.59
5268964-26896499.20299.86
6275679-275679101.679102.36
45min1265865-26586598.059100.292.1398.89101.132.13
2280901-280901103.605104.47
3274103-274103101.098101.94
4267275-26727598.57999.40
5268275-26827598.94899.77
6275118-275118101.472102.32
极限1266422-26642298.265100.181.9899.25101.181.98
2279886-279886103.231104.27
3274536-274536101.257102.27
4267151-26715198.53399.52
5267726-26772698.74699.74
6273903-273903101.024102.04
点击查看处理图标(自动生成)
 
原始图谱下载图谱(姜进硙 于 2024-08-14 16:08:15 完成)
生成报告数据部分(等待生成报告)
Current page cost:70 ms